ethylthio-8 methyl-5 5H-dibenzazepine-10-acetate de nitro-4 phenyle

Base Information

Chemical Name:ethylthio-8 methyl-5 5H-dibenzazepine-10-acetate de nitro-4 phenyle
CAS No.:52813-87-3
Molecular Formula:C₂₅H₂₂N₂O₄S
Molecular Weight:446.527
Hs Code.:

ethylthio-8 methyl-5 5H-dibenz<b,f>azepine-10-acetate de nitro-4 phenyle

Synonyms:ethylthio-8 methyl-5 5H-dibenzazepine-10-acetate de nitro-4 phenyle

Suppliers and Price of ethylthio-8 methyl-5 5H-dibenzazepine-10-acetate de nitro-4 phenyle

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of ethylthio-8 methyl-5 5H-dibenzazepine-10-acetate de nitro-4 phenyle

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

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Technology Process of ethylthio-8 methyl-5 5H-dibenzazepine-10-acetate de nitro-4 phenyle

There total 7 articles about ethylthio-8 methyl-5 5H-dibenzazepine-10-acetate de nitro-4 phenyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 52813-86-2
(8-Ethylsulfanyl-5-methyl-5H-dibenzo[b,f]azepin-10-yl)-acetic acid

: 52813-87-3
ethylthio-8 methyl-5 5H-dibenzazepine-10-acetate de nitro-4 phenyle

Guidance literature:: With dicyclohexyl-carbodiimide; In ethyl acetate; for 1.5h; Heating;

Reference yield:

: 52813-81-7
bromo-8 dihydro-5,11 methyl-5 10H-dibenzazepine-10-one

: 52813-87-3
ethylthio-8 methyl-5 5H-dibenzazepine-10-acetate de nitro-4 phenyle

Guidance literature:: Multi-step reaction with 6 steps

1: 100 percent / TsOH / ethanol / 1.5 h / 70 °C

2: 99 percent / pyridine, quinoline / 5 h / Heating

3: Zn / tetrahydrofuran / 4 h / 10 °C

4: 2N HCl / methanol / 4 h

5: 80 percent / KOH / ethanol / 2 h

6: 87 percent / dicyclohexyl carbodiimide / ethyl acetate / 1.5 h / Heating

With pyridine; quinoline; hydrogenchloride; potassium hydroxide; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; zinc; In tetrahydrofuran; methanol; ethanol; ethyl acetate;

Reference yield:

: 52813-83-9
ethylthio-8 dihydro-5,11 methyl-5 10H-dibenzazepine-10-one

: 52813-87-3
ethylthio-8 methyl-5 5H-dibenzazepine-10-acetate de nitro-4 phenyle

Guidance literature:: Multi-step reaction with 4 steps

1: Zn / tetrahydrofuran / 4 h / 10 °C

2: 2N HCl / methanol / 4 h

3: 80 percent / KOH / ethanol / 2 h

4: 87 percent / dicyclohexyl carbodiimide / ethyl acetate / 1.5 h / Heating

With hydrogenchloride; potassium hydroxide; dicyclohexyl-carbodiimide; zinc; In tetrahydrofuran; methanol; ethanol; ethyl acetate;