2,4-dimethoxybenzyl 3-methanesulfonyloxy-2-methoxy-2-methyl-3-phenylpropionate

Base Information

Chemical Name:2,4-dimethoxybenzyl 3-methanesulfonyloxy-2-methoxy-2-methyl-3-phenylpropionate
CAS No.:503073-66-3
Molecular Formula:C₂₁H₂₆O₈S
Molecular Weight:438.499
Hs Code.:

Synonyms:2,4-dimethoxybenzyl 3-methanesulfonyloxy-2-methoxy-2-methyl-3-phenylpropionate

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Chemical Property of 2,4-dimethoxybenzyl 3-methanesulfonyloxy-2-methoxy-2-methyl-3-phenylpropionate

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Technology Process of 2,4-dimethoxybenzyl 3-methanesulfonyloxy-2-methoxy-2-methyl-3-phenylpropionate

There total 1 articles about 2,4-dimethoxybenzyl 3-methanesulfonyloxy-2-methoxy-2-methyl-3-phenylpropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 124-63-0
methanesulfonyl chloride

: 343986-64-1
2,4-dimethoxybenzyl 3-hydroxy-2-methoxy-2-methyl-3-phenylpropionate

: 503073-66-3
2,4-dimethoxybenzyl 3-methanesulfonyloxy-2-methoxy-2-methyl-3-phenylpropionate

Guidance literature:: With pyridine;
DOI:10.1021/ol034061o

Reference yield:

: 503073-66-3
2,4-dimethoxybenzyl 3-methanesulfonyloxy-2-methoxy-2-methyl-3-phenylpropionate

: 503073-67-4
3-methanesulfonyloxy-2-methoxy-2-methyl-3-phenylpropionic acid

Guidance literature:: With ammonium cerium(IV) nitrate; In water; acetonitrile; at 20 ℃; for 1h;
DOI:10.1021/ol034061o

Reference yield:

: 503073-66-3
2,4-dimethoxybenzyl 3-methanesulfonyloxy-2-methoxy-2-methyl-3-phenylpropionate

: C₁₀H₁₁O

Guidance literature:: Multi-step reaction with 3 steps

1: cerium(IV) ammonium nitrate / acetonitrile; H₂O / 1 h / 20 °C

2: 0.59 g / triethylamine / CH₂Cl₂ / 0 - 20 °C

3: acetonitrile / Flash photolysis

With ammonium cerium(IV) nitrate; triethylamine; In dichloromethane; water; acetonitrile;
DOI:10.1021/ol034061o