4-(diethoxyphosphorylmethyl)-N,N-bis[4-(diethoxyphosphorylmethyl)phenyl]aniline

Base Information

Chemical Name:4-(diethoxyphosphorylmethyl)-N,N-bis[4-(diethoxyphosphorylmethyl)phenyl]aniline
CAS No.:245653-28-5
Molecular Formula:C₃₃H₄₈NO₉P₃
Molecular Weight:695.667
Hs Code.:2921499090
DSSTox Substance ID:DTXSID00454504
Nikkaji Number:J1.954.279C
Wikidata:Q82276063
Mol file:245653-28-5.mol

Synonyms:245653-28-5;4-(diethoxyphosphorylmethyl)-N,N-bis[4-(diethoxyphosphorylmethyl)phenyl]aniline;Diethyl (4-{bis-[4-(diethoxy-phosphorylmethyl)-phenyl]-amino}-benzyl)-phosphonate;Phosphonic acid, P,P',P''-[nitrilotris(4,1-phenylenemethylene)]tris-, P,P,P',P',P'',P''-hexaethyl ester;DTXSID00454504;Tris[4-(diethoxyphosphinylmethyl)phenyl]amine;Hexaethyl {nitrilotris[(4,1-phenylene)methylene]}tris(phosphonate)

Suppliers and Price of 4-(diethoxyphosphorylmethyl)-N,N-bis[4-(diethoxyphosphorylmethyl)phenyl]aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(4-(BIS-[4-(DIETHOXY-PHOSPHORYLMETHYL)-PHENYL]-AMINO)-BENZYL)-PHOSPHONIC ACID DIETHYL ESTER 95.00%
1G
$ 1064.79

Total 5 raw suppliers

Chemical Property of 4-(diethoxyphosphorylmethyl)-N,N-bis[4-(diethoxyphosphorylmethyl)phenyl]aniline

Chemical Property:

PSA：139.26000
LogP:10.45470
XLogP3:4.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:10
Rotatable Bond Count:21
Exact Mass:695.25419310
Heavy Atom Count:46
Complexity:839

Purity/Quality:

98% ^*data from raw suppliers

(4-(BIS-[4-(DIETHOXY-PHOSPHORYLMETHYL)-PHENYL]-AMINO)-BENZYL)-PHOSPHONIC ACID DIETHYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOP(=O)(CC1=CC=C(C=C1)N(C2=CC=C(C=C2)CP(=O)(OCC)OCC)C3=CC=C(C=C3)CP(=O)(OCC)OCC)OCC

Technology Process of 4-(diethoxyphosphorylmethyl)-N,N-bis[4-(diethoxyphosphorylmethyl)phenyl]aniline

There total 4 articles about 4-(diethoxyphosphorylmethyl)-N,N-bis[4-(diethoxyphosphorylmethyl)phenyl]aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 78-40-0
triethyl phosphate

: N,N,N-tris(4-bromomethylbenzen-1-yl)amine

: 245653-28-5
tris(4-diethylphosphonatemethylphenyl)amine

Guidance literature:: at 120 ℃; Inert atmosphere;
DOI:10.1002/chem.201200849

Reference yield: 59.0%

: 122-52-1
triethyl phosphite

: N,N,N-tris(4-bromomethylbenzen-1-yl)amine

: 245653-28-5
tris(4-diethylphosphonatemethylphenyl)amine

Guidance literature:: for 72h; Heating;
DOI:10.1016/j.tetlet.2003.09.025

Reference yield:

: 119001-43-3
tris(4-formylphenyl)amine

: 245653-28-5
tris(4-diethylphosphonatemethylphenyl)amine

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / KBH₄ / ethanol; CH₂Cl₂ / 5 h / 20 °C

2: 85 percent / HBr / H₂O / 5 h / Heating

3: 59 percent / 72 h / Heating

With potassium borohydride; hydrogen bromide; In ethanol; dichloromethane; water; 3: Michaelis-Arbuzov reaction;
DOI:10.1016/j.tetlet.2003.09.025