isopropyl 2-azido-2-deoxy-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranozide

Base Information

Chemical Name:isopropyl 2-azido-2-deoxy-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranozide
CAS No.:866552-40-1
Molecular Formula:C₂₃H₂₇N₃O₅
Molecular Weight:425.484
Hs Code.:

Synonyms:isopropyl 2-azido-2-deoxy-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranozide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of isopropyl 2-azido-2-deoxy-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranozide

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Technology Process of isopropyl 2-azido-2-deoxy-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranozide

There total 3 articles about isopropyl 2-azido-2-deoxy-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranozide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 67-63-0,8013-70-5
isopropyl alcohol

: 310870-37-2
O-(2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α,β-D-glucopyranosyl) trichloroacetimidate

: 866552-40-1
isopropyl 2-azido-2-deoxy-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranozide

: isopropyl 2-azido-2-deoxy-3-O-benzyl-4,6-O-benzylidene-α-D-glucopyranozide

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere; Molecular sieve;
DOI:10.1002/chem.201202770

Reference yield:

: 67-63-0,8013-70-5
isopropyl alcohol

: 245110-00-3
2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl trichloroacetimidate

: 866552-40-1
isopropyl 2-azido-2-deoxy-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranozide

: isopropyl 2-azido-2-deoxy-3-O-benzyl-4,6-O-benzylidene-α-D-glucopyranozide

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate; at 20 ℃; for 48h;
DOI:10.1021/jo050704x

Reference yield:

: 67-63-0,8013-70-5
isopropyl alcohol

: 2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-glucopyranosyl trichloroacetimidate

: 866552-40-1
isopropyl 2-azido-2-deoxy-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranozide

: isopropyl 2-azido-2-deoxy-3-O-benzyl-4,6-O-benzylidene-α-D-glucopyranozide

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 1-ethyl-3-methylimidazolium triflate; at 20 ℃; for 1h;
DOI:10.1021/jo050704x