1-Hexanesulfonamide

Base Information

• Chemical Name: 1-Hexanesulfonamide
• CAS No.: 3144-11-4
• Molecular Formula: C6H15 N O2 S
• Molecular Weight: 165.257
• Hs Code.: 2935009090
• Mol file: 3144-11-4.mol

Synonyms:Hexanesulfonamide

Chemical Property of 1-Hexanesulfonamide

Chemical Property:

• PSA: 68.54000
• LogP: 2.63630

Purity/Quality:

98% ^*data from raw suppliers

1-HEXANESULFONAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Hexanesulfonamide

There total 4 articles about 1-Hexanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1-hexanesulfonyl chloride (14532-24-2) → 1-hexanesulfonamide (3144-11-4)

Guidance literature:

With ammonia; In ethyl acetate; at 0 - 20 ℃; for 0.75h;

DOI:10.1016/j.ejmech.2009.11.052

Reference yield: 84.0%

→ 1-hexanesulfonamide (3144-11-4)

Guidance literature:

Reference yield: 55.0%

1-bromo-hexane (111-25-1) → 1-hexanesulfonamide (3144-11-4)

Guidance literature:

1-bromo-hexane; With sodium sulfite; In water; Heating;

With trichlorophosphate; at 130 ℃; for 4h;

With ammonia; In water; acetonitrile; at 0 ℃; for 1h;

DOI:10.1002/hlca.200490148

upstream raw materials:

1-hexanesulfonyl chloride

1-bromo-hexane

1-hexylthiocyanate

Downstream raw materials:

4-(biphenyl-4-ylmethylsulfanylmethyl)-N-(hexane-1-sulfonyl)benzoylamide

N-[[(4-chlorophenyl)amino]carbonyl]-1-hexanesulfonamide

Trianilinophosphazosulfonylhexyl

N--hexan-sulfonimidsaeure-(1)-<4-nitro-phenylester>

Refernces

• 1、 -. "Pharmaceutical Compositions Based on Fluorinated Sulphamides and Sulphinimides". Page/Page column 9. . Retrieved 2008/06/13.
• 2、 -. "5(Z)-7-(endo-3-benzenesulfonamidobicyclo[2.2.1]hept-exo-2-yl)-5-heptenoic acid, sodium salt". . . Retrieved 2008/06/13.