2-13C-2-thiophenyl ethanol

Base Information

Chemical Name:2-13C-2-thiophenyl ethanol
CAS No.:169518-58-5
Molecular Formula:C₈H₁₀OS
Molecular Weight:155.222
Hs Code.:

Synonyms:2-13C-2-thiophenyl ethanol

Suppliers and Price of 2-13C-2-thiophenyl ethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-13C-2-thiophenyl ethanol

Chemical Property:

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Technology Process of 2-13C-2-thiophenyl ethanol

There total 2 articles about 2-13C-2-thiophenyl ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 169518-57-4
methyl 1-13C-2-thiophenyl acetate

: 169518-58-5
2-13C-2-thiophenyl ethanol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 - 20 ℃;
DOI:10.1002/jlcr.2580360707

Reference yield:

: 108-98-5
thiophenol

: 169518-58-5
2-13C-2-thiophenyl ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaOMe / 1.) RT, 30 min, 2.) reflux, 40 min

2: 94 percent / LiAlH₄ / diethyl ether / 0 - 20 °C

With lithium aluminium tetrahydride; sodium methylate; In diethyl ether;
DOI:10.1002/jlcr.2580360707

Reference yield:

: 169518-58-5
2-13C-2-thiophenyl ethanol

: 1-13C-2-chloroethyl phenyl sulfide

: 2-13C-2-chloroethyl phenyl sulfide

Guidance literature:: With thionyl chloride; In dichloromethane; for 2h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;
DOI:10.1002/jlcr.2580360707