(1S,2S,6S,7R)-2,6,8,9-Tetramethyl-3,10-diphenyl-3,10-diphospha-tricyclo[5.2.1.0^2,6]deca-4,8-diene 3,10-dioxide

Base Information

• Chemical Name: (1S,2S,6S,7R)-2,6,8,9-Tetramethyl-3,10-diphenyl-3,10-diphospha-tricyclo[5.2.1.0^2,6]deca-4,8-diene 3,10-dioxide
• CAS No.: 126958-87-0
• Molecular Formula: C₂₄H₂₆O₂P₂
• Molecular Weight: 408.417

Synonyms:(1S,2S,6S,7R)-2,6,8,9-Tetramethyl-3,10-diphenyl-3,10-diphospha-tricyclo[5.2.1.0^2,6]deca-4,8-diene 3,10-dioxide

Chemical Property of (1S,2S,6S,7R)-2,6,8,9-Tetramethyl-3,10-diphenyl-3,10-diphospha-tricyclo[5.2.1.0^2,6]deca-4,8-diene 3,10-dioxide

Chemical Property:

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Technology Process of (1S,2S,6S,7R)-2,6,8,9-Tetramethyl-3,10-diphenyl-3,10-diphospha-tricyclo[5.2.1.0^2,6]deca-4,8-diene 3,10-dioxide

There total 2 articles about (1S,2S,6S,7R)-2,6,8,9-Tetramethyl-3,10-diphenyl-3,10-diphospha-tricyclo[5.2.1.0^2,6]deca-4,8-diene 3,10-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzonitrile oxide (873-67-6) + 3,4-dimethyl-1-phenylphosphole (30540-36-4) → benzonitrile (100-47-0) + (1S,2S,6S,7R)-2,6,8,9-Tetramethyl-3,10-diphenyl-3,10-diphospha-tricyclo[5.2.1.02,6]deca-4,8-diene 3,10-dioxide (126958-87-0)

Guidance literature:

In diethyl ether; at 0 ℃;

DOI:10.1016/S0040-4020(01)89176-6

Reference yield:

3,4-dimethyl-1-phenylphosphole (30540-36-4) + diazodiphenylmethane (908093-98-1) → (1S,2S,6S,7R)-2,6,8,9-Tetramethyl-3,10-diphenyl-3,10-diphospha-tricyclo[5.2.1.02,6]deca-4,8-diene 3,10-dioxide (126958-87-0)

Guidance literature:

With oxygen; In diethyl ether; at 25 ℃; for 24h; under 750.06 Torr;

DOI:10.1016/S0040-4020(01)89176-6

upstream raw materials:

benzonitrile oxide

3,4-dimethyl-1-phenylphosphole

diazodiphenylmethane

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