N-(6-bromo-2-methoxy-3-(benzyloxy)benzylidene)-6,7-(methylenedioxy)-1-naphthylamine

Base Information

Chemical Name:N-(6-bromo-2-methoxy-3-(benzyloxy)benzylidene)-6,7-(methylenedioxy)-1-naphthylamine
CAS No.:113250-74-1
Molecular Formula:C₂₆H₂₀BrNO₄
Molecular Weight:490.353
Hs Code.:

Synonyms:N-(6-bromo-2-methoxy-3-(benzyloxy)benzylidene)-6,7-(methylenedioxy)-1-naphthylamine

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Chemical Property of N-(6-bromo-2-methoxy-3-(benzyloxy)benzylidene)-6,7-(methylenedioxy)-1-naphthylamine

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Technology Process of N-(6-bromo-2-methoxy-3-(benzyloxy)benzylidene)-6,7-(methylenedioxy)-1-naphthylamine

There total 11 articles about N-(6-bromo-2-methoxy-3-(benzyloxy)benzylidene)-6,7-(methylenedioxy)-1-naphthylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 53811-49-7
naphtho[2,3-d][1,3]dioxol-5-amine

: 95712-55-3
2-methoxy-3-(benzyloxy)-6-bromobenzaldehyde

: 113250-74-1
N-(6-bromo-2-methoxy-3-(benzyloxy)benzylidene)-6,7-(methylenedioxy)-1-naphthylamine

Guidance literature:: at 160 - 170 ℃; for 2h;
DOI:10.1021/jo00243a020

Reference yield:

: 24677-78-9
2,3-dihydroxybenzaldehyde

: 113250-74-1
N-(6-bromo-2-methoxy-3-(benzyloxy)benzylidene)-6,7-(methylenedioxy)-1-naphthylamine

Guidance literature:: Multi-step reaction with 7 steps

1: 1.) NaH / 1.) DMSO, 70 deg C, 1 h, 2.) DMSO, 70 deg C, 1 h

2: 98.8 percent / triethylamine / benzene / 2 h

3: Br₂, KBr / H₂O

4: 55.5 percent / 10percent aq. NaOH

5: 62 percent / 33percent aq. HCl / acetone / 10 h / Heating

6: 91 percent / K₂CO₃ / acetone / 5 h / Heating

7: 98 percent / 2 h / 160 - 170 °C

With hydrogenchloride; sodium hydroxide; bromine; sodium hydride; potassium carbonate; triethylamine; potassium bromide; In water; acetone; benzene;
DOI:10.1021/jo00243a020

Reference yield:

: 86734-59-0
3-benzyloxy-2-hydroxybenzaldehyde

: 113250-74-1
N-(6-bromo-2-methoxy-3-(benzyloxy)benzylidene)-6,7-(methylenedioxy)-1-naphthylamine

Guidance literature:: Multi-step reaction with 6 steps

1: 98.8 percent / triethylamine / benzene / 2 h

2: Br₂, KBr / H₂O

3: 55.5 percent / 10percent aq. NaOH

4: 62 percent / 33percent aq. HCl / acetone / 10 h / Heating

5: 91 percent / K₂CO₃ / acetone / 5 h / Heating

6: 98 percent / 2 h / 160 - 170 °C

With hydrogenchloride; sodium hydroxide; bromine; potassium carbonate; triethylamine; potassium bromide; In water; acetone; benzene;
DOI:10.1021/jo00243a020