2,3,4-Tri-O-acetyl-1<(benzoyl)(phenyl)amino>-1-desoxy-β-D-glucopyranuronsaeure-methylester

Base Information

Chemical Name:2,3,4-Tri-O-acetyl-1<(benzoyl)(phenyl)amino>-1-desoxy-β-D-glucopyranuronsaeure-methylester
CAS No.:96622-75-2
Molecular Formula:C₂₆H₂₇NO₁₀
Molecular Weight:513.501
Hs Code.:

Synonyms:2,3,4-Tri-O-acetyl-1<(benzoyl)(phenyl)amino>-1-desoxy-β-D-glucopyranuronsaeure-methylester

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Chemical Property of 2,3,4-Tri-O-acetyl-1<(benzoyl)(phenyl)amino>-1-desoxy-β-D-glucopyranuronsaeure-methylester

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Technology Process of 2,3,4-Tri-O-acetyl-1<(benzoyl)(phenyl)amino>-1-desoxy-β-D-glucopyranuronsaeure-methylester

There total 2 articles about 2,3,4-Tri-O-acetyl-1<(benzoyl)(phenyl)amino>-1-desoxy-β-D-glucopyranuronsaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 96622-71-8
N-Phenylbenzimidsaeure-trimethylsilylester

: 7355-18-2
(2S,3S,4S,5R,6S)-3,4,5,6-Tetraacetoxy-tetrahydro-pyran-2-carboxylic acid methyl ester

: 96622-75-2
2,3,4-Tri-O-acetyl-1<(benzoyl)(phenyl)amino>-1-desoxy-β-D-glucopyranuronsaeure-methylester

Guidance literature:: With molecular sieve; trimethylsilyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 60 ℃; for 8h;

Reference yield:

: 93-98-1,5705-51-1
N-phenyl benzoyl amide

: 96622-75-2
2,3,4-Tri-O-acetyl-1<(benzoyl)(phenyl)amino>-1-desoxy-β-D-glucopyranuronsaeure-methylester

Guidance literature:: Multi-step reaction with 2 steps

1: 1) LiN(iPr)2 / 1) THF, -78 deg C, 30 min; 2) 8 h, room temp.

2: 85 percent / molecular sieve, trifluoromethanesulfonic acid trimethylsilylester / 1,2-dichloro-ethane / 8 h / 60 °C

With molecular sieve; trimethylsilyl trifluoromethanesulfonate; lithium diisopropyl amide; In 1,2-dichloro-ethane;