(S)-3-tert-butoxycarbonyl-3-[(N-benzyloxycarbonyl-N-methyl)amino]propanoylsuccinimide

Base Information

Chemical Name:(S)-3-tert-butoxycarbonyl-3-[(N-benzyloxycarbonyl-N-methyl)amino]propanoylsuccinimide
CAS No.:765299-29-4
Molecular Formula:C₂₁H₂₆N₂O₈
Molecular Weight:434.446
Hs Code.:

Synonyms:(S)-3-tert-butoxycarbonyl-3-[(N-benzyloxycarbonyl-N-methyl)amino]propanoylsuccinimide

Suppliers and Price of (S)-3-tert-butoxycarbonyl-3-[(N-benzyloxycarbonyl-N-methyl)amino]propanoylsuccinimide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-3-tert-butoxycarbonyl-3-[(N-benzyloxycarbonyl-N-methyl)amino]propanoylsuccinimide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-3-tert-butoxycarbonyl-3-[(N-benzyloxycarbonyl-N-methyl)amino]propanoylsuccinimide

There total 3 articles about (S)-3-tert-butoxycarbonyl-3-[(N-benzyloxycarbonyl-N-methyl)amino]propanoylsuccinimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: 765299-28-3
1-tert-butyl (S)-N-benzyloxycarbonyl-N-methylaspartate

: 765299-29-4
(S)-3-tert-butoxycarbonyl-3-[(N-benzyloxycarbonyl-N-methyl)amino]propanoylsuccinimide

Guidance literature:: With dicyclohexyl-carbodiimide; In 1,4-dioxane; ethyl acetate; at 5 ℃;
DOI:10.1016/j.tet.2004.06.034

Reference yield:

: 60079-12-1
β-Methyl α-tert-butyl (2S)-N-(benzyloxycarbonyl)aspartate

: 765299-29-4
(S)-3-tert-butoxycarbonyl-3-[(N-benzyloxycarbonyl-N-methyl)amino]propanoylsuccinimide

Guidance literature:: Multi-step reaction with 3 steps

1: Ag₂O / dimethylformamide / 7 h / 20 °C

2: LiOH*H₂O / aq. methanol / 5 - 20 °C

3: 97 percent / N,N'-dicyclohexylcarbodiimide / dioxane; ethyl acetate / 5 °C

With lithium hydroxide; dicyclohexyl-carbodiimide; silver(l) oxide; In 1,4-dioxane; methanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2004.06.034

Reference yield:

: 765299-27-2
1-tert-butyl methyl (S)-N-benzyloxycarbonyl-N-methylaspartate

: 765299-29-4
(S)-3-tert-butoxycarbonyl-3-[(N-benzyloxycarbonyl-N-methyl)amino]propanoylsuccinimide

Guidance literature:: Multi-step reaction with 2 steps

1: LiOH*H₂O / aq. methanol / 5 - 20 °C

2: 97 percent / N,N'-dicyclohexylcarbodiimide / dioxane; ethyl acetate / 5 °C

With lithium hydroxide; dicyclohexyl-carbodiimide; In 1,4-dioxane; methanol; ethyl acetate;
DOI:10.1016/j.tet.2004.06.034