Propane-1-sulfinic acid 1-phenyl-meth-(E)-ylideneamide

Base Information

• Chemical Name: Propane-1-sulfinic acid 1-phenyl-meth-(E)-ylideneamide
• CAS No.: 871939-95-6
• Molecular Formula: C₁₀H₁₃NOS
• Molecular Weight: 195.285
• Mol file: 871939-95-6.mol

Synonyms:Propane-1-sulfinic acid 1-phenyl-meth-(E)-ylideneamide

Chemical Property of Propane-1-sulfinic acid 1-phenyl-meth-(E)-ylideneamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Propane-1-sulfinic acid 1-phenyl-meth-(E)-ylideneamide

There total 1 articles about Propane-1-sulfinic acid 1-phenyl-meth-(E)-ylideneamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

propane-1-sulfinamide (871939-84-3) + benzaldehyde (100-52-7) → Propane-1-sulfinic acid 1-phenyl-meth-(E)-ylideneamide (871939-95-6)

Guidance literature:

With titanium(IV) tetraethanolate; In dichloromethane; Heating;

DOI:10.1021/ol052250w

Reference yield:

Propane-1-sulfinic acid 1-phenyl-meth-(E)-ylideneamide (871939-95-6) → N-Benzylidenepropane-1-sulfonamide

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃;

DOI:10.1021/ol052250w

Reference yield:

Propane-1-sulfinic acid 1-phenyl-meth-(E)-ylideneamide (871939-95-6) → 3-phenyl-2-n-propylsulfonyloxaziridine

Guidance literature:

Multi-step reaction with 2 steps

1: 3-chloro-peroxybenzoic acid / CH₂Cl₂ / 20 °C

2: 3-chloro-peroxybenzoic acid; KOH / CH₂Cl₂ / 0.02 h / 20 °C

With potassium hydroxide; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

DOI:10.1021/ol052250w

upstream raw materials:

propane-1-sulfinamide

benzaldehyde