diethyldithiocarbamic acid [(4-methoxybenzyl)(cyclohex-2-enyl)carbamic acid]thioanhydride

Base Information

• Chemical Name: diethyldithiocarbamic acid [(4-methoxybenzyl)(cyclohex-2-enyl)carbamic acid]thioanhydride
• CAS No.: 1373492-50-2
• Molecular Formula: C₂₀H₂₈N₂O₂S₂
• Molecular Weight: 392.587

Synonyms:diethyldithiocarbamic acid [(4-methoxybenzyl)(cyclohex-2-enyl)carbamic acid]thioanhydride

Chemical Property of diethyldithiocarbamic acid [(4-methoxybenzyl)(cyclohex-2-enyl)carbamic acid]thioanhydride

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Technology Process of diethyldithiocarbamic acid [(4-methoxybenzyl)(cyclohex-2-enyl)carbamic acid]thioanhydride

There total 4 articles about diethyldithiocarbamic acid [(4-methoxybenzyl)(cyclohex-2-enyl)carbamic acid]thioanhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

cyclohex-2-en-1-yl(4-methoxybenzyl)carbamic chloride (1373492-69-3) + sodium diethyldithiocarbamate trihydrate (20624-25-3) → diethyldithiocarbamic acid [(4-methoxybenzyl)(cyclohex-2-enyl)carbamic acid]thioanhydride (1373492-50-2)

Guidance literature:

In acetone; at 20 ℃; for 18h; Inert atmosphere;

DOI:10.1021/ol300605y

Reference yield:

rac-3-bromocyclohexene (1521-51-3,113667-32-6) → diethyldithiocarbamic acid [(4-methoxybenzyl)(cyclohex-2-enyl)carbamic acid]thioanhydride (1373492-50-2)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 8 h / 20 °C / Inert atmosphere

2: pyridine / toluene / 18 h / 20 °C / Inert atmosphere

3: acetone / 18 h / 20 °C / Inert atmosphere

With pyridine; potassium carbonate; In acetone; toluene; acetonitrile;

DOI:10.1021/ol300605y

Reference yield:

4-methoxy-benzylamine (2393-23-9) → diethyldithiocarbamic acid [(4-methoxybenzyl)(cyclohex-2-enyl)carbamic acid]thioanhydride (1373492-50-2)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 8 h / 20 °C / Inert atmosphere

2: pyridine / toluene / 18 h / 20 °C / Inert atmosphere

3: acetone / 18 h / 20 °C / Inert atmosphere

With pyridine; potassium carbonate; In acetone; toluene; acetonitrile;

DOI:10.1021/ol300605y

upstream raw materials:

cyclohex-2-en-1-yl(4-methoxybenzyl)carbamic chloride

sodium diethyldithiocarbamate trihydrate

4-methoxy-benzylamine

rac-3-bromocyclohexene

Downstream raw materials:

(+/-)-7-(4-methoxybenzyl)-7-azabicyclo[4.2.0]oct-1-en-8-one

(±)-(1R,6S)-7-(4-methoxyphenyl)-7-azabicyclo[4.2.0]oct-2-en-8-one

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