[2-(2,6-dichloro-phenylamino-[4-D])-phenyl-[3,4,5,6-D₄]]-essigs?ure-[1,1-D₂]

Base Information

• Chemical Name: [2-(2,6-dichloro-phenylamino-[4-D])-phenyl-[3,4,5,6-D₄]]-essigs?ure-[1,1-D₂]
• CAS No.: 1401311-57-6
• Molecular Formula: C₁₄H₁₁Cl₂NO₂
• Molecular Weight: 303.097

Synonyms:[2-(2,6-dichloro-phenylamino-[4-D])-phenyl-[3,4,5,6-D₄]]-essigs?ure-[1,1-D₂]

Chemical Property of [2-(2,6-dichloro-phenylamino-[4-D])-phenyl-[3,4,5,6-D₄]]-essigs?ure-[1,1-D₂]

Chemical Property:

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Technology Process of [2-(2,6-dichloro-phenylamino-[4-D])-phenyl-[3,4,5,6-D₄]]-essigs?ure-[1,1-D₂]

There total 4 articles about [2-(2,6-dichloro-phenylamino-[4-D])-phenyl-[3,4,5,6-D₄]]-essigs?ure-[1,1-D₂] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

[2-(2,6-dichloroanilino)phenyl]acetic acid (15307-86-5) → [2-(2,6-dichloro-phenylamino-[4-D])-phenyl-[3,4,5,6-D4]]-essigs?ure-[1,1-D2] (1401311-57-6,153466-65-0)

Guidance literature:

With [D]-sodium hydroxide; deuteromethanol; In water-d2; at 130 ℃; for 0.00277778h; Inert atmosphere; Microwave irradiation; Sealed tube;

DOI:10.1002/jlcr.3103

Reference yield: 65.0%

1-(2,6-dichlorophenyl-[4-D])-1,3-dihydro-indol-2-one-[3,3,4,5,6,7-D6] (1401311-51-0) → [2-(2,6-dichloro-phenylamino-[4-D])-phenyl-[3,4,5,6-D4]]-essigs?ure-[1,1-D2] (1401311-57-6,153466-65-0)

Guidance literature:

With [D]-sodium hydroxide; deuteromethanol; In water-d2; at 130 ℃; for 0.00277778h; Inert atmosphere; Microwave irradiation;

DOI:10.1016/j.bmc.2012.06.052

Reference yield:

diclofenac sodium (15307-79-6) → [2-(2,6-dichloro-phenylamino-[4-D])-phenyl-[3,4,5,6-D4]]-essigs?ure-[1,1-D2] (1401311-57-6,153466-65-0)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrogen chloride; water-d2 / 0.33 h / 160 °C / Microwave irradiation

2: potassium tetrachloroplatinate(II); water-d2; deuteroacetic acid / 0.33 h / 160 °C / Inert atmosphere; Microwave irradiation

3: deuteromethanol; [D]-sodium hydroxide / water-d2 / 0 h / 130 °C / Inert atmosphere; Microwave irradiation

With potassium tetrachloroplatinate(II); [D]-sodium hydroxide; deuteromethanol; deuteroacetic acid; water-d2; hydrogen chloride; In water-d2;

DOI:10.1016/j.bmc.2012.06.052

upstream raw materials:

diclofenac sodium

1-(2,6-dichlorophenyl)-1,3-dihydro-indol-2-one-[3,3,5,7-D₄]

1-(2,6-dichlorophenyl-[4-D])-1,3-dihydro-indol-2-one-[3,3,4,5,6,7-D₆]

[2-(2,6-dichloroanilino)phenyl]acetic acid

Downstream raw materials:

[2-(2,6-dichloro-4-hydroxyphenylamino)-phenyl-[3,4,5,6-D₄]]-essigs?ure-[1,1-D₂]

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