C₄₀H₅₇N₃O₁₀Si₂

Base Information Edit

Chemical Name:C₄₀H₅₇N₃O₁₀Si₂
CAS No.:182201-65-6
Molecular Formula:C₄₀H₅₇N₃O₁₀Si₂
Molecular Weight:796.078
Hs Code.:
Mol file:182201-65-6.mol

C<sub>40</sub>H<sub>57</sub>N<sub>3</sub>O<sub>10</sub>Si<sub>2</sub>

Synonyms:C₄₀H₅₇N₃O₁₀Si₂

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Chemical Property of C₄₀H₅₇N₃O₁₀Si₂ Edit

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Technology Process of C₄₀H₅₇N₃O₁₀Si₂

There total 18 articles about C₄₀H₅₇N₃O₁₀Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 151-50-8
potassium cyanide

: 182201-52-1
C₁₃H₁₃NO₅

: 182201-56-5
{(S)-2-[3,5-Bis-(tert-butyl-dimethyl-silanyloxy)-4-methoxy-phenyl]-1-formyl-ethyl}-carbamic acid allyl ester

: 182201-65-6
C₄₀H₅₇N₃O₁₀Si₂

Guidance literature:: With acetic acid; at 23 ℃; for 18h;
DOI:10.1021/ja962480t

Reference yield:

: 111726-43-3
3,4-(methylenedioxy)phenyl methoxymethyl ether

: 182201-65-6
C₄₀H₅₇N₃O₁₀Si₂

Guidance literature:: Multi-step reaction with 13 steps

1: 1.) BuLi, tetramethylethylene diamine / 1.) hexane, 0 deg C, 4 h, 2.) hexane, from -78 deg C to 23 deg C, 15 min

2: 1.) BuLi / 1.) THF, -30 deg C, 13 h

3: CH₃SO₃H / CH₂Cl₂ / 0 °C

4: 1.) NaH / 1.) DMF, 0 deg C, 5 min, 2.) DMF, 23 deg C, 40 min

5: 99 percent / piperidine, acetic acid / benzene / 18 h / 23 °C

6: 94 percent / Et₃N, HCOOH, Pd(PPh₃)4 / 4 h / 23 °C

7: (PhO)2P(O)N₃, Et₃N, 4 Angstroem molecular sieves / toluene / 2 h / 70 °C

8: 1 h / 23 °C

9: 97 percent / H₂, Rh<(COD)-(R,R)-DIPAMP>(+)*BF₄(-) / 16 h / 23 °C / 2280 Torr

10: BF₃*Et₂O, H₂O / CH₂Cl₂ / 0.17 h / 0 °C

11: BF₃*Et₂O, 4 Angstroem molecular sieves / CH₂Cl₂ / 18 h / 23 °C

12: 100 percent / H₂ / 10percent Pd/C / ethyl acetate / 6 h / 23 °C / 760 Torr

13: 61 percent / HOAc / 18 h / 23 °C

With piperidine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; formic acid; methanesulfonic acid; N,N,N,N,-tetramethylethylenediamine; Rh<(COD)-(R,R)-DIPAMP>(+)*BF4(-); 4 A molecular sieve; diphenyl phosphoryl azide; boron trifluoride diethyl etherate; water; hydrogen; sodium hydride; acetic acid; triethylamine; palladium on activated charcoal; In dichloromethane; ethyl acetate; toluene; benzene;
DOI:10.1021/ja962480t

Reference yield:

: 187040-02-4
5-methoxy methoxy-4-methyl benzo[d][1,3]dioxole

: 182201-65-6
C₄₀H₅₇N₃O₁₀Si₂

Guidance literature:: Multi-step reaction with 12 steps

1: 1.) BuLi / 1.) THF, -30 deg C, 13 h

2: CH₃SO₃H / CH₂Cl₂ / 0 °C

3: 1.) NaH / 1.) DMF, 0 deg C, 5 min, 2.) DMF, 23 deg C, 40 min

4: 99 percent / piperidine, acetic acid / benzene / 18 h / 23 °C

5: 94 percent / Et₃N, HCOOH, Pd(PPh₃)4 / 4 h / 23 °C

6: (PhO)2P(O)N₃, Et₃N, 4 Angstroem molecular sieves / toluene / 2 h / 70 °C

7: 1 h / 23 °C

8: 97 percent / H₂, Rh<(COD)-(R,R)-DIPAMP>(+)*BF₄(-) / 16 h / 23 °C / 2280 Torr

9: BF₃*Et₂O, H₂O / CH₂Cl₂ / 0.17 h / 0 °C

10: BF₃*Et₂O, 4 Angstroem molecular sieves / CH₂Cl₂ / 18 h / 23 °C

11: 100 percent / H₂ / 10percent Pd/C / ethyl acetate / 6 h / 23 °C / 760 Torr

12: 61 percent / HOAc / 18 h / 23 °C

With piperidine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; formic acid; methanesulfonic acid; Rh<(COD)-(R,R)-DIPAMP>(+)*BF4(-); 4 A molecular sieve; diphenyl phosphoryl azide; boron trifluoride diethyl etherate; water; hydrogen; sodium hydride; acetic acid; triethylamine; palladium on activated charcoal; In dichloromethane; ethyl acetate; toluene; benzene;
DOI:10.1021/ja962480t