6-ethyl-1-[3,4-bis(benzoxy)phenyl]-2-benzylcarbamate-2,3,4,9-tetrahydro-1H-β-carboline

Base Information

Chemical Name:6-ethyl-1-[3,4-bis(benzoxy)phenyl]-2-benzylcarbamate-2,3,4,9-tetrahydro-1H-β-carboline
CAS No.:1310575-40-6
Molecular Formula:C₄₁H₃₈N₂O₄
Molecular Weight:622.764
Hs Code.:

Synonyms:6-ethyl-1-[3,4-bis(benzoxy)phenyl]-2-benzylcarbamate-2,3,4,9-tetrahydro-1H-β-carboline

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Chemical Property of 6-ethyl-1-[3,4-bis(benzoxy)phenyl]-2-benzylcarbamate-2,3,4,9-tetrahydro-1H-β-carboline

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Technology Process of 6-ethyl-1-[3,4-bis(benzoxy)phenyl]-2-benzylcarbamate-2,3,4,9-tetrahydro-1H-β-carboline

There total 5 articles about 6-ethyl-1-[3,4-bis(benzoxy)phenyl]-2-benzylcarbamate-2,3,4,9-tetrahydro-1H-β-carboline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 6-ethyl-1-[3,4-bis(benzoxy)phenyl]-2,3,4,9-tetrahydro-1H-β-carboline hydrochloride

: 501-53-1,94274-21-2
benzyl chloroformate

: 1310575-40-6
6-ethyl-1-[3,4-bis(benzoxy)phenyl]-2-benzylcarbamate-2,3,4,9-tetrahydro-1H-β-carboline

Guidance literature:: With potassium carbonate; In water; ethyl acetate; at 0 - 20 ℃; for 3h;
DOI:10.1016/j.ejmech.2011.03.048

Reference yield:

: 136281-75-9
(5-ethyl-1H-indol-3-yl)acetonitrile

: 1310575-40-6
6-ethyl-1-[3,4-bis(benzoxy)phenyl]-2-benzylcarbamate-2,3,4,9-tetrahydro-1H-β-carboline

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / diethyl ether

2: trifluoroacetic acid / dichloromethane / 24 h / 20 °C

3: potassium carbonate / water; ethyl acetate / 3 h / 0 - 20 °C

With lithium aluminium tetrahydride; potassium carbonate; trifluoroacetic acid; In diethyl ether; dichloromethane; water; ethyl acetate;
DOI:10.1016/j.ejmech.2011.03.048

Reference yield:

: 54840-34-5
(4-ethylphenyl)hydrazine

: 1310575-40-6
6-ethyl-1-[3,4-bis(benzoxy)phenyl]-2-benzylcarbamate-2,3,4,9-tetrahydro-1H-β-carboline

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid

2: lithium aluminium tetrahydride / diethyl ether

3: trifluoroacetic acid / dichloromethane / 24 h / 20 °C

4: potassium carbonate / water; ethyl acetate / 3 h / 0 - 20 °C

With lithium aluminium tetrahydride; sulfuric acid; potassium carbonate; trifluoroacetic acid; In diethyl ether; dichloromethane; water; ethyl acetate;
DOI:10.1016/j.ejmech.2011.03.048