(±)-4-(3-chlorophenyl)-2-(4-nitrophenoxy)-1,3,2-dioxaphosphinane-2-oxide

Base Information

Chemical Name:(±)-4-(3-chlorophenyl)-2-(4-nitrophenoxy)-1,3,2-dioxaphosphinane-2-oxide
CAS No.:883989-27-3
Molecular Formula:C₁₅H₁₃ClNO₆P
Molecular Weight:369.698
Hs Code.:

Synonyms:(±)-4-(3-chlorophenyl)-2-(4-nitrophenoxy)-1,3,2-dioxaphosphinane-2-oxide

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Chemical Property of (±)-4-(3-chlorophenyl)-2-(4-nitrophenoxy)-1,3,2-dioxaphosphinane-2-oxide

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Technology Process of (±)-4-(3-chlorophenyl)-2-(4-nitrophenoxy)-1,3,2-dioxaphosphinane-2-oxide

There total 8 articles about (±)-4-(3-chlorophenyl)-2-(4-nitrophenoxy)-1,3,2-dioxaphosphinane-2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51699-45-7
(S)-(-)-1-(3'-Chlorophenyl)-1,3-Propanediol

: 883989-27-3
(±)-4-(3-chlorophenyl)-2-(4-nitrophenoxy)-1,3,2-dioxaphosphinane-2-oxide

Guidance literature:: (S)-(-)-1-(3'-Chlorophenyl)-1,3-Propanediol; With sodium hydroxide; ammonium chloride; triethylamine; trichlorophosphate; In dichloromethane; at 0 ℃; for 2h;

With 4-nitrophenol sodium salt; In tetrahydrofuran; dichloromethane; for 4h; Heating / reflux;

Reference yield:

: 805235-83-0
(4R)-(+)-trans-2-(4-nitrophenoxy)-2-oxo-4-(3-chlorophenyl)-1,3,2-dioxaphosphorinane

: 883989-27-3
(±)-4-(3-chlorophenyl)-2-(4-nitrophenoxy)-1,3,2-dioxaphosphinane-2-oxide

Guidance literature:: With lithium 4-nitrophenolate; In tetrahydrofuran; at 20 ℃; for 5h;

Reference yield:

: 777-52-6
1-dichlorophosphoryloxy-4-nitro-benzene

: 625095-57-0
(S)-(-)-1-(3-Chlorophenyl)-1,3-propanediol

: 883989-27-3
(±)-4-(3-chlorophenyl)-2-(4-nitrophenoxy)-1,3,2-dioxaphosphinane-2-oxide

Guidance literature:: 1-dichlorophosphoryloxy-4-nitro-benzene; (S)-(-)-1-(3-Chlorophenyl)-1,3-propanediol; With triethylamine; In tetrahydrofuran; at 20 ℃; for 2h; Heating / reflux;

With 4-nitrophenol sodium salt; at 20 - 30 ℃; for 3.5h; Heating / reflux;