ethyl 1-(4'-(5-(((2-methoxy-1-phenylethoxy)carbonyl)amino)-1-methyl-1H-pyrazol-4-yl)-[1,1 '-biphenyl]-4-yl)cyclopropanecarboxylate

Base Information

Chemical Name:ethyl 1-(4'-(5-(((2-methoxy-1-phenylethoxy)carbonyl)amino)-1-methyl-1H-pyrazol-4-yl)-[1,1 '-biphenyl]-4-yl)cyclopropanecarboxylate
CAS No.:1402466-13-0
Molecular Formula:C₃₂H₃₃N₃O₅
Molecular Weight:539.631
Hs Code.:

Synonyms:ethyl 1-(4'-(5-(((2-methoxy-1-phenylethoxy)carbonyl)amino)-1-methyl-1H-pyrazol-4-yl)-[1,1 '-biphenyl]-4-yl)cyclopropanecarboxylate

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Chemical Property of ethyl 1-(4'-(5-(((2-methoxy-1-phenylethoxy)carbonyl)amino)-1-methyl-1H-pyrazol-4-yl)-[1,1 '-biphenyl]-4-yl)cyclopropanecarboxylate

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Technology Process of ethyl 1-(4'-(5-(((2-methoxy-1-phenylethoxy)carbonyl)amino)-1-methyl-1H-pyrazol-4-yl)-[1,1 '-biphenyl]-4-yl)cyclopropanecarboxylate

There total 2 articles about ethyl 1-(4'-(5-(((2-methoxy-1-phenylethoxy)carbonyl)amino)-1-methyl-1H-pyrazol-4-yl)-[1,1 '-biphenyl]-4-yl)cyclopropanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1380587-87-0
1-[4'-(5-amino-1-methyl-1H-pyrazol-4-yl)-biphenyl-4-yl]-cyclopropanecarboxylic acid ethyl ester

: 3587-84-6
2-methoxy-1-phenylethanol

: 503-38-8
trichloromethyl chloroformate

: 1402466-13-0
ethyl 1-(4'-(5-(((2-methoxy-1-phenylethoxy)carbonyl)amino)-1-methyl-1H-pyrazol-4-yl)-[1,1 '-biphenyl]-4-yl)cyclopropanecarboxylate

Guidance literature:: 1-[4'-(5-amino-1-methyl-1H-pyrazol-4-yl)-biphenyl-4-yl]-cyclopropanecarboxylic acid ethyl ester; trichloromethyl chloroformate; With pyridine; In dichloromethane; at 20 ℃; for 0.5h;

2-methoxy-1-phenylethanol; In dichloromethane; at 20 ℃; for 36h;

Reference yield:

: 4079-52-1
methoxymethyl phenyl ketone

: 1402466-13-0
ethyl 1-(4'-(5-(((2-methoxy-1-phenylethoxy)carbonyl)amino)-1-methyl-1H-pyrazol-4-yl)-[1,1 '-biphenyl]-4-yl)cyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tetrahydroborate; methanol / 1 h / 0 - 20 °C

2.1: pyridine / dichloromethane / 0.5 h / 20 °C

2.2: 36 h / 20 °C

With pyridine; methanol; sodium tetrahydroborate; In dichloromethane;

Reference yield:

: 1402466-13-0
ethyl 1-(4'-(5-(((2-methoxy-1-phenylethoxy)carbonyl)amino)-1-methyl-1H-pyrazol-4-yl)-[1,1 '-biphenyl]-4-yl)cyclopropanecarboxylate

: 1402465-55-7
1-(4'-(5-((2-methoxy-1-phenylethoxy)carbonylamino)-1-methyl-1H-pyrazol-4-yl)biphenyl-4-yl)cyclopropane-1-carboxylic acid

Guidance literature:: ethyl 1-(4'-(5-(((2-methoxy-1-phenylethoxy)carbonyl)amino)-1-methyl-1H-pyrazol-4-yl)-[1,1 '-biphenyl]-4-yl)cyclopropanecarboxylate; With lithium hydroxide monohydrate; water; In tetrahydrofuran; water; at 20 ℃; for 2h;

With hydrogenchloride; In tetrahydrofuran; methanol; water;