1-tert-Butoxy-2c-hydroxymethyl-2t-methyl-3c-phenyl-1r-cyclopropancarbonsaeure-lacton

Base Information

Chemical Name:1-tert-Butoxy-2c-hydroxymethyl-2t-methyl-3c-phenyl-1r-cyclopropancarbonsaeure-lacton
CAS No.:77301-70-3
Molecular Formula:C₁₆H₂₀O₃
Molecular Weight:260.333
Hs Code.:

Synonyms:1-tert-Butoxy-2c-hydroxymethyl-2t-methyl-3c-phenyl-1r-cyclopropancarbonsaeure-lacton

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-tert-Butoxy-2c-hydroxymethyl-2t-methyl-3c-phenyl-1r-cyclopropancarbonsaeure-lacton

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Technology Process of 1-tert-Butoxy-2c-hydroxymethyl-2t-methyl-3c-phenyl-1r-cyclopropancarbonsaeure-lacton

There total 4 articles about 1-tert-Butoxy-2c-hydroxymethyl-2t-methyl-3c-phenyl-1r-cyclopropancarbonsaeure-lacton which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 865-47-4
potassium tert-butylate

: 77301-67-8
1-Chlor-c-2-(hydroxymethyl)-t-2-methyl-t-3-phenyl-r-1-cyclopropancarbonsaeurelacton

: 77301-70-3
1-tert-Butoxy-2c-hydroxymethyl-2t-methyl-3c-phenyl-1r-cyclopropancarbonsaeure-lacton

Guidance literature:: In tetrahydrofuran; 1) 15 min, 0 deg C, 2) 45 min, r.t.;

Reference yield: 92.0%

: 865-47-4
potassium tert-butylate

: 77301-67-8,77341-61-8
1-Chlor-2c-hydroxymethyl-2t-methyl-3c-phenyl-1r-cyclopropancarbonsaeure-lacton

: 77301-70-3
1-tert-Butoxy-2c-hydroxymethyl-2t-methyl-3c-phenyl-1r-cyclopropancarbonsaeure-lacton

Guidance literature:: In tetrahydrofuran; 1) 15 min, 0 deg C, 2) 45 min, r.t.;

Reference yield:

: 77301-64-5,77341-59-4,100163-46-0,100163-47-1
2,2-Dichlor-1-methyl-t-3-phenyl-r-1-cyclopropanmethanol-tetrahydro-2-pyranylether

: 77301-70-3
1-tert-Butoxy-2c-hydroxymethyl-2t-methyl-3c-phenyl-1r-cyclopropancarbonsaeure-lacton

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 15percent n-BuLi / 1) hexane, THF, benzine, -105 deg C, 1 h, 2) hexane, THF, benzine, r.t.

2: 92 percent / tetrahydrofuran / 1) 15 min, 0 deg C, 2) 45 min, r.t.

With n-butyllithium; In tetrahydrofuran;