[3-[1-(benzenesulfonyl)indol-3-yl]allyl] 3-(4-methoxyphenyl)prop-2-ynoate

Base Information

• Chemical Name: [3-[1-(benzenesulfonyl)indol-3-yl]allyl] 3-(4-methoxyphenyl)prop-2-ynoate
• CAS No.: 1256752-41-6
• Molecular Formula: C₂₇H₂₁NO₅S
• Molecular Weight: 471.533

Synonyms:[3-[1-(benzenesulfonyl)indol-3-yl]allyl] 3-(4-methoxyphenyl)prop-2-ynoate

Chemical Property of [3-[1-(benzenesulfonyl)indol-3-yl]allyl] 3-(4-methoxyphenyl)prop-2-ynoate

Chemical Property:

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Technology Process of [3-[1-(benzenesulfonyl)indol-3-yl]allyl] 3-(4-methoxyphenyl)prop-2-ynoate

There total 1 articles about [3-[1-(benzenesulfonyl)indol-3-yl]allyl] 3-(4-methoxyphenyl)prop-2-ynoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

3-(4-methoxyphenyl)propynoic acid (2227-57-8) + 1-benzenesulphonyl-3-(3-chloroprop-1-en-1-yl)-1H-indole (1022988-04-0) → [3-[1-(benzenesulfonyl)indol-3-yl]allyl] 3-(4-methoxyphenyl)prop-2-ynoate (1256752-41-6)

Guidance literature:

3-(4-methoxyphenyl)propynoic acid; With sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 20 ℃; for 1h; Inert atmosphere; Darkness;

1-benzenesulphonyl-3-(3-chloroprop-1-en-1-yl)-1H-indole; In N,N-dimethyl-formamide; at 20 ℃; for 48h; Inert atmosphere; Darkness;

DOI:10.1016/j.ejmech.2010.09.003

Reference yield: 88.0%

[3-[1-(benzenesulfonyl)indol-3-yl]allyl] 3-(4-methoxyphenyl)prop-2-ynoate (1256752-41-6) → 5-benzenesulphonyl-4-(4-methoxyphenyl)-1,5-dihydro-3H-furo[3,4-b]carbazol-3-one (1256752-51-8)

Guidance literature:

[3-[1-(benzenesulfonyl)indol-3-yl]allyl] 3-(4-methoxyphenyl)prop-2-ynoate; In toluene; at 150 ℃; for 1h; Microwave irradiation;

With o-tetrachloroquinone; In toluene; at 150 ℃; for 0.583333h; Microwave irradiation;

DOI:10.1016/j.ejmech.2010.09.003

Reference yield: 81.0%

[3-[1-(benzenesulfonyl)indol-3-yl]allyl] 3-(4-methoxyphenyl)prop-2-ynoate (1256752-41-6) → 4-(4-methoxyphenyl)-5-benzenesulphonyl-1H-furo[3,4-b]carbazol-3(3H,5H,10H)-one (1256752-46-1)

Guidance literature:

In toluene; at 150 ℃; for 2.5h; Microwave irradiation;

DOI:10.1016/j.ejmech.2010.09.003

upstream raw materials:

3-(4-methoxyphenyl)propynoic acid

1-benzenesulphonyl-3-(3-chloroprop-1-en-1-yl)-1H-indole

Downstream raw materials:

4-(4-methoxyphenyl)-5-benzenesulphonyl-1H-furo[3,4-b]carbazol-3(3H,5H,10H)-one

5-benzenesulphonyl-4-(4-methoxyphenyl)-1,5-dihydro-3H-furo[3,4-b]carbazol-3-one

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