2-hydroxy-4-methylcetophenone ethoxycarbonylhydrazone

Base Information

Chemical Name:2-hydroxy-4-methylcetophenone ethoxycarbonylhydrazone
CAS No.:529487-11-4
Molecular Formula:C₁₂H₁₆N₂O₃
Molecular Weight:236.271
Hs Code.:

Synonyms:2-hydroxy-4-methylcetophenone ethoxycarbonylhydrazone

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Chemical Property of 2-hydroxy-4-methylcetophenone ethoxycarbonylhydrazone

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Technology Process of 2-hydroxy-4-methylcetophenone ethoxycarbonylhydrazone

There total 1 articles about 2-hydroxy-4-methylcetophenone ethoxycarbonylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 6921-64-8
4'-hydroxy-2'-methylacetophenone

: 4114-31-2
ethylhydrazine carboxylate

: 529487-11-4
2-hydroxy-4-methylcetophenone ethoxycarbonylhydrazone

Guidance literature:: With acetic acid; In ethanol; for 0.5h; Heating;
DOI:10.1023/A:1022568808446

Reference yield: 87.0%

: 529487-11-4
2-hydroxy-4-methylcetophenone ethoxycarbonylhydrazone

: 529487-12-5
4-(2-hydroxy-4-methylphenyl)-1,2,3-thiadiazole

Guidance literature:: With thionyl chloride; at 60 ℃; for 1h;
DOI:10.1023/A:1022568808446

Reference yield:

: 529487-11-4
2-hydroxy-4-methylcetophenone ethoxycarbonylhydrazone

: 2-(2,4-dinitrophenylthio)-6-methylbenzofuran

Guidance literature:: Multi-step reaction with 2 steps

1.1: 87 percent / thionyl chloride / 1 h / 60 °C

2.1: K₂CO₃ / acetonitrile / 0.5 h / Heating

2.2: 59 percent / acetonitrile / 4 h / Heating

With thionyl chloride; potassium carbonate; In acetonitrile;
DOI:10.1023/A:1022568808446