2-(3-benzyloxycarbonylamino-3-ethoxycarbonylpropyl)thiazol-5-carboxylic acid

Base Information

Chemical Name:2-(3-benzyloxycarbonylamino-3-ethoxycarbonylpropyl)thiazol-5-carboxylic acid
CAS No.:683742-39-4
Molecular Formula:C₁₈H₂₀N₂O₆S
Molecular Weight:392.433
Hs Code.:

Synonyms:2-(3-benzyloxycarbonylamino-3-ethoxycarbonylpropyl)thiazol-5-carboxylic acid

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Chemical Property of 2-(3-benzyloxycarbonylamino-3-ethoxycarbonylpropyl)thiazol-5-carboxylic acid

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Technology Process of 2-(3-benzyloxycarbonylamino-3-ethoxycarbonylpropyl)thiazol-5-carboxylic acid

There total 1 articles about 2-(3-benzyloxycarbonylamino-3-ethoxycarbonylpropyl)thiazol-5-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: t-butyl 2-(3-benzyloxycarbonylamino-3-ethoxycarbonylpropyl)thiazol-5-carboxylate hydrochloride

: 683742-39-4
2-(3-benzyloxycarbonylamino-3-ethoxycarbonylpropyl)thiazol-5-carboxylic acid

Guidance literature:: With trifluoroacetic acid; for 2h; Ambient temperature;
DOI:10.1016/0223-5234(93)90125-X

Reference yield:

: 541-41-3
chloroformic acid ethyl ester

: 683742-39-4
2-(3-benzyloxycarbonylamino-3-ethoxycarbonylpropyl)thiazol-5-carboxylic acid

: 2-Benzyloxycarbonylamino-4-(4-ethoxycarbonyloxycarbonyl-thiazol-2-yl)-butyric acid ethyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran; at -15 ℃; for 0.133333h;
DOI:10.1016/0223-5234(93)90125-X

Reference yield:

: 683742-39-4
2-(3-benzyloxycarbonylamino-3-ethoxycarbonylpropyl)thiazol-5-carboxylic acid

: methyl N-(2-(3-benzyloxycarbonylamino-3-ethoxycarbonylpropyl)thiazol-5-carbonyl)glycinate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / tetrahydrofuran / 0.13 h / -15 °C

2: Et₃N / tetrahydrofuran / Ambient temperature

With triethylamine; In tetrahydrofuran;
DOI:10.1016/0223-5234(93)90125-X