(1'S,2'S,2R)-2-(diethoxymethyl)-2-<1'-benzyloxy-2',3'-<(1-methylethylidene)dioxy>propoxy>oxirane

Base Information

Chemical Name:(1'S,2'S,2R)-2-(diethoxymethyl)-2-<1'-benzyloxy-2',3'-<(1-methylethylidene)dioxy>propoxy>oxirane
CAS No.:171016-34-5
Molecular Formula:C₂₀H₃₀O₆
Molecular Weight:366.455
Hs Code.:

Synonyms:(1'S,2'S,2R)-2-(diethoxymethyl)-2-<1'-benzyloxy-2',3'-<(1-methylethylidene)dioxy>propoxy>oxirane

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Chemical Property of (1'S,2'S,2R)-2-(diethoxymethyl)-2-<1'-benzyloxy-2',3'-<(1-methylethylidene)dioxy>propoxy>oxirane

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Technology Process of (1'S,2'S,2R)-2-(diethoxymethyl)-2-<1'-benzyloxy-2',3'-<(1-methylethylidene)dioxy>propoxy>oxirane

There total 2 articles about (1'S,2'S,2R)-2-(diethoxymethyl)-2-<1'-benzyloxy-2',3'-<(1-methylethylidene)dioxy>propoxy>oxirane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 100-39-0
benzyl bromide

: 171231-62-2
(1'S,2'S,2R)-2-(diethoxymethyl)-2-<1'-hydroxy-2',3'-<(1-methylethylidene)dioxy>propoxy>oxirane

: 171016-34-5
(1'S,2'S,2R)-2-(diethoxymethyl)-2-<1'-benzyloxy-2',3'-<(1-methylethylidene)dioxy>propoxy>oxirane

Guidance literature:: With sodium hydride; In dimethyl sulfoxide;
DOI:10.1016/0040-4020(95)00680-7

Reference yield:

: 171484-84-7
(3R,4S)-2-(diethoxymethyl)-4,5-<(1-methylethylidene)dioxy>pent-1-en-3-ol

: 171016-34-5
(1'S,2'S,2R)-2-(diethoxymethyl)-2-<1'-benzyloxy-2',3'-<(1-methylethylidene)dioxy>propoxy>oxirane

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / VO(acac), t-BuOOH / benzene; toluene / Ambient temperature

2: 80 percent / NaH / dimethylsulfoxide

With tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium; sodium hydride; In dimethyl sulfoxide; toluene; benzene;
DOI:10.1016/0040-4020(95)00680-7