Ni(CO)2(SiCl₂(1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene))2

Base Information

• Chemical Name: Ni(CO)2(SiCl₂(1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene))2
• CAS No.: 1254164-29-8
• Molecular Formula: C₅₆H₇₂Cl₄N₄NiO₂Si₂
• Molecular Weight: 1089.89
• Mol file: 1254164-29-8.mol

Synonyms:Ni(CO)2(SiCl₂(1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene))2

Chemical Property of Ni(CO)2(SiCl₂(1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene))2

Chemical Property:

Purity/Quality:

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Technology Process of Ni(CO)2(SiCl₂(1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene))2

There total 1 articles about Ni(CO)2(SiCl₂(1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene))2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

IPr*SiCl2 (1187680-47-2) + tetracarbonyl nickel (13463-39-3,71564-36-8) → Ni(CO)2(SiCl2(1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene))2 (1254164-29-8)

Guidance literature:

In diethyl ether; toluene; byproducts: CO; (N2); addn. of ethereal soln. of nickel compd. to toluene soln. of silylene deriv. at room temp., stirring for 12 h; filtration through celite, concg., keeping at room temp. overnight, isolation of crystals, elem. anal.;

DOI:10.1021/ic101556s

upstream raw materials:

IPr*SiCl₂

tetracarbonyl nickel