(dimethylamino)(phenyl)methylidene-tetrafluoro[4-(4-propylcyclohexyl)phenyl]phosphorane

Base Information

Chemical Name:(dimethylamino)(phenyl)methylidene-tetrafluoro[4-(4-propylcyclohexyl)phenyl]phosphorane
CAS No.:1455481-90-9
Molecular Formula:C₂₄H₃₂F₄NP
Molecular Weight:441.492
Hs Code.:

Synonyms:(dimethylamino)(phenyl)methylidene-tetrafluoro[4-(4-propylcyclohexyl)phenyl]phosphorane

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Chemical Property of (dimethylamino)(phenyl)methylidene-tetrafluoro[4-(4-propylcyclohexyl)phenyl]phosphorane

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Technology Process of (dimethylamino)(phenyl)methylidene-tetrafluoro[4-(4-propylcyclohexyl)phenyl]phosphorane

There total 5 articles about (dimethylamino)(phenyl)methylidene-tetrafluoro[4-(4-propylcyclohexyl)phenyl]phosphorane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 702-99-8
α,α-difluoro0N,N-dimethylbenzylamine

: 1455481-70-5
dichloro[4-(4-propylcyclohexyl)phenyl]phosphine

: 1455481-90-9
(dimethylamino)(phenyl)methylidene-tetrafluoro[4-(4-propylcyclohexyl)phenyl]phosphorane

Guidance literature:: In tetrahydrofuran; at -40 - 20 ℃; for 18h; Inert atmosphere;
DOI:10.1016/j.tet.2013.07.062

Reference yield:

: 611-74-5
N,N-dimethylbenzamide

: 1455481-90-9
(dimethylamino)(phenyl)methylidene-tetrafluoro[4-(4-propylcyclohexyl)phenyl]phosphorane

Guidance literature:: Multi-step reaction with 2 steps

1.1: Carbonyl fluoride / acetonitrile / 20 °C / Inert atmosphere

1.2: Heating; Inert atmosphere

2.1: tetrahydrofuran / 18 h / -40 - 20 °C / Inert atmosphere

With Carbonyl fluoride; In tetrahydrofuran; acetonitrile;
DOI:10.1016/j.tet.2013.07.062

Reference yield:

: 86579-53-5,167858-55-1
4-(4-propylcyclohexyl)-1-bromobenzene

: 1455481-90-9
(dimethylamino)(phenyl)methylidene-tetrafluoro[4-(4-propylcyclohexyl)phenyl]phosphorane

Guidance literature:: Multi-step reaction with 4 steps

1: magnesium / tetrahydrofuran / 1 h / Inert atmosphere; Reflux

2: tetrahydrofuran / 16 h / -20 - 20 °C / Inert atmosphere

3: hydrogenchloride / diethyl ether / 20 °C / Inert atmosphere

4: tetrahydrofuran / 18 h / -40 - 20 °C / Inert atmosphere

With hydrogenchloride; magnesium; In tetrahydrofuran; diethyl ether;
DOI:10.1016/j.tet.2013.07.062