(4S)-methyl 2,2-dioxo-3-(9-(9-phenylfluorenyl))-1,2,3-oxathiazolidine-4-carboxylate

Base Information

Chemical Name:(4S)-methyl 2,2-dioxo-3-(9-(9-phenylfluorenyl))-1,2,3-oxathiazolidine-4-carboxylate
CAS No.:296774-94-2
Molecular Formula:C₂₃H₁₉NO₅S
Molecular Weight:421.474
Hs Code.:

Synonyms:(4S)-methyl 2,2-dioxo-3-(9-(9-phenylfluorenyl))-1,2,3-oxathiazolidine-4-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S)-methyl 2,2-dioxo-3-(9-(9-phenylfluorenyl))-1,2,3-oxathiazolidine-4-carboxylate

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Technology Process of (4S)-methyl 2,2-dioxo-3-(9-(9-phenylfluorenyl))-1,2,3-oxathiazolidine-4-carboxylate

There total 1 articles about (4S)-methyl 2,2-dioxo-3-(9-(9-phenylfluorenyl))-1,2,3-oxathiazolidine-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: (2RS,4S)-methyl 2-oxo-3-(9-phenylfluoren-9-yl)-1,2,3-oxathiazolidine-4-carboxylate

: 296774-94-2
(4S)-methyl 2,2-dioxo-3-(9-(9-phenylfluorenyl))-1,2,3-oxathiazolidine-4-carboxylate

Guidance literature:: With ruthenium trichloride; sodium periodate; In water; acetonitrile; at 0 ℃; for 4h;
DOI:10.1139/v00-176

Reference yield: 87.0%

: Na-Salz des Acetessigsaeure-methylester

: 296774-94-2
(4S)-methyl 2,2-dioxo-3-(9-(9-phenylfluorenyl))-1,2,3-oxathiazolidine-4-carboxylate

: methyl 1-N-(9-phenylfluoren-9-yl)-2-methyl-3-[(methyloxy)carbonyl]-Δ²-pyrroline

Guidance literature:: (4S)-methyl 2,2-dioxo-3-(9-(9-phenylfluorenyl))-1,2,3-oxathiazolidine-4-carboxylate; With sodium hydride; In 1,2-dimethoxyethane; at 20 ℃; for 0.5h;

Na-Salz des Acetessigsaeure-methylester; In 1,2-dimethoxyethane; for 18h; Heating;
DOI:10.1139/v00-176

Reference yield: 86.0%

: 105-45-3
acetoacetic acid methyl ester

: 296774-94-2
(4S)-methyl 2,2-dioxo-3-(9-(9-phenylfluorenyl))-1,2,3-oxathiazolidine-4-carboxylate

: 296774-83-9
methyl 5-oxo-4-(methyloxycarbonyl)-2-[N-(9-phenylfluoren-9-yl)amino]hexanoate

Guidance literature:: acetoacetic acid methyl ester; With sodium hydride; In 1,2-dimethoxyethane; for 0.166667h;

(4S)-methyl 2,2-dioxo-3-(9-(9-phenylfluorenyl))-1,2,3-oxathiazolidine-4-carboxylate; In 1,2-dimethoxyethane; at 60 ℃; for 18h;
DOI:10.1139/v00-176