{[3-bromo-1-(2-bromo-4-chlorophenyl)propyl]oxy}(1,1-dimethylethyl)dimethylsilane

Base Information

Chemical Name:{[3-bromo-1-(2-bromo-4-chlorophenyl)propyl]oxy}(1,1-dimethylethyl)dimethylsilane
CAS No.:1378432-50-8
Molecular Formula:C₁₅H₂₃Br₂ClOSi
Molecular Weight:442.694
Hs Code.:

Synonyms:{[3-bromo-1-(2-bromo-4-chlorophenyl)propyl]oxy}(1,1-dimethylethyl)dimethylsilane

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Chemical Property of {[3-bromo-1-(2-bromo-4-chlorophenyl)propyl]oxy}(1,1-dimethylethyl)dimethylsilane

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Technology Process of {[3-bromo-1-(2-bromo-4-chlorophenyl)propyl]oxy}(1,1-dimethylethyl)dimethylsilane

There total 1 articles about {[3-bromo-1-(2-bromo-4-chlorophenyl)propyl]oxy}(1,1-dimethylethyl)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1378432-47-3
3-(2-bromo-4-chlorophenyl)-3-{[(1,1-dimethylethyl)(dimethyl)silyl]oxy}-1-propanol

: 1378432-50-8
{[3-bromo-1-(2-bromo-4-chlorophenyl)propyl]oxy}(1,1-dimethylethyl)dimethylsilane

Guidance literature:: With N-Bromosuccinimide; triphenylphosphine; In dichloromethane; at 0 - 20 ℃;

Reference yield: 87.0%

: 691856-35-6
5-cyclopropyl-2-(4-fluorophenyl)-N-methyl-6-(methylsulfonamido)benzofuran-3-carboxamide

: 1378432-50-8
{[3-bromo-1-(2-bromo-4-chlorophenyl)propyl]oxy}(1,1-dimethylethyl)dimethylsilane

: 1378432-52-0
6-[(3-(2-bromo-4-chlorophenyl)-3-{[(1,1-dimethylethyl)(dimethyl)silyl]oxy}propyl)(methylsulfonyl)amino]-5-cyclopropyl-2-(4-fluorophenyl)-N-methyl-1-benzofuran-3-carboxamide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; acetonitrile; at 75 - 85 ℃; for 51h;

Reference yield:

: 1378432-50-8
{[3-bromo-1-(2-bromo-4-chlorophenyl)propyl]oxy}(1,1-dimethylethyl)dimethylsilane

: 1378428-24-0
6-[[2-(5-chloro-1-hydroxy-1,3-dihydro-2,1-benzoxaborol-3-yl)ethyl](methylsulfonyl)amino]-5-cyclopropyl-2-(4-fluorophenyl)-N-methyl-1-benzofuran-3-carboxamide

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / N,N-dimethyl-formamide; acetonitrile / 51 h / 75 - 85 °C

2: hydrogenchloride / water; tetrahydrofuran / 19 h / 55 °C / Reflux

3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 40 h / 50 - 55 °C

4: potassium acetate; sodium bromide / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 64 h / 85 °C

5: hydrogenchloride / water; tetrahydrofuran / 20 h / Reflux

With hydrogenchloride; potassium acetate; potassium carbonate; N-ethyl-N,N-diisopropylamine; sodium bromide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide; acetonitrile;