3-(4-(9H-carbazol-9-yl)phenyl)-5-(3,5-di-tert-butyl-4-methoxyphenyl)-5-oxopentanoic acid

Base Information

Chemical Name:3-(4-(9H-carbazol-9-yl)phenyl)-5-(3,5-di-tert-butyl-4-methoxyphenyl)-5-oxopentanoic acid
CAS No.:1367364-25-7
Molecular Formula:C₃₈H₄₁NO₄
Molecular Weight:575.748
Hs Code.:

Synonyms:3-(4-(9H-carbazol-9-yl)phenyl)-5-(3,5-di-tert-butyl-4-methoxyphenyl)-5-oxopentanoic acid

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Chemical Property of 3-(4-(9H-carbazol-9-yl)phenyl)-5-(3,5-di-tert-butyl-4-methoxyphenyl)-5-oxopentanoic acid

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Technology Process of 3-(4-(9H-carbazol-9-yl)phenyl)-5-(3,5-di-tert-butyl-4-methoxyphenyl)-5-oxopentanoic acid

There total 7 articles about 3-(4-(9H-carbazol-9-yl)phenyl)-5-(3,5-di-tert-butyl-4-methoxyphenyl)-5-oxopentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1610365-79-1
C₃₉H₄₁NO₆

: 1367364-25-7
3-(4-(9H-carbazol-9-yl)phenyl)-5-(3,5-di-tert-butyl-4-methoxyphenyl)-5-oxopentanoic acid

Guidance literature:: With hydrogenchloride; In water; acetic acid; for 6h; Reflux;

Reference yield:

: 86-74-8,105184-46-1,97960-57-1
9H-carbazole

: 1367364-25-7
3-(4-(9H-carbazol-9-yl)phenyl)-5-(3,5-di-tert-butyl-4-methoxyphenyl)-5-oxopentanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: copper; potassium carbonate / nitrobenzene / 6 h / Inert atmosphere; Reflux

2: sodium hydroxide / ethanol / 20 °C

3: potassium hydroxide / ethanol; dichloromethane / 6 h / Reflux

4: potassium hydroxide / water; acetone / 20 °C

5: acetic acid; hydrogenchloride / water / Reflux

With hydrogenchloride; copper; potassium carbonate; acetic acid; potassium hydroxide; sodium hydroxide; In ethanol; dichloromethane; water; nitrobenzene; acetone; 1: |Ullmann Condensation / 2: |Aldol Condensation / 3: |Michael Addition;
DOI:10.1002/cmdc.201400007

Reference yield:

: 1122-91-4
4-bromo-benzaldehyde

: 1367364-25-7
3-(4-(9H-carbazol-9-yl)phenyl)-5-(3,5-di-tert-butyl-4-methoxyphenyl)-5-oxopentanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: copper; potassium carbonate / nitrobenzene / 6 h / Inert atmosphere; Reflux

2: sodium hydroxide / ethanol / 20 °C

3: potassium hydroxide / ethanol; dichloromethane / 6 h / Reflux

4: potassium hydroxide / water; acetone / 20 °C

5: acetic acid; hydrogenchloride / water / Reflux

With hydrogenchloride; copper; potassium carbonate; acetic acid; potassium hydroxide; sodium hydroxide; In ethanol; dichloromethane; water; nitrobenzene; acetone; 1: |Ullmann Condensation / 2: |Aldol Condensation / 3: |Michael Addition;
DOI:10.1002/cmdc.201400007