di-tert-butul 2-(4-[4-(4-[1,3-bis(tert-butoxycarbonyl)tetrahydro-1H-2-imidazolyliden]aminophenyl)piperazino]phenylimino)-1,3-imidazolidinedicarboxylate

Base Information

Chemical Name:di-tert-butul 2-(4-[4-(4-[1,3-bis(tert-butoxycarbonyl)tetrahydro-1H-2-imidazolyliden]aminophenyl)piperazino]phenylimino)-1,3-imidazolidinedicarboxylate
CAS No.:692259-85-1
Molecular Formula:C₄₂H₆₀N₈O₈
Molecular Weight:804.987
Hs Code.:

di-tert-butul 2-(4-[4-(4-[1,3-bis(tert-butoxycarbonyl)tetrahydro-1H-2-imidazolyliden]aminophenyl)piperazino]phenylimino)-1,3-imidazolidinedicarboxylate

Synonyms:di-tert-butul 2-(4-[4-(4-[1,3-bis(tert-butoxycarbonyl)tetrahydro-1H-2-imidazolyliden]aminophenyl)piperazino]phenylimino)-1,3-imidazolidinedicarboxylate

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Chemical Property of di-tert-butul 2-(4-[4-(4-[1,3-bis(tert-butoxycarbonyl)tetrahydro-1H-2-imidazolyliden]aminophenyl)piperazino]phenylimino)-1,3-imidazolidinedicarboxylate

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Technology Process of di-tert-butul 2-(4-[4-(4-[1,3-bis(tert-butoxycarbonyl)tetrahydro-1H-2-imidazolyliden]aminophenyl)piperazino]phenylimino)-1,3-imidazolidinedicarboxylate

There total 4 articles about di-tert-butul 2-(4-[4-(4-[1,3-bis(tert-butoxycarbonyl)tetrahydro-1H-2-imidazolyliden]aminophenyl)piperazino]phenylimino)-1,3-imidazolidinedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 173300-83-9
2-thioxo-imidazolidine-1,3-dicarboxylic acid di-tert-butyl ester

: 1,4-bis(4-aminophenyl)piperazine hydrochloride salt

: 692259-85-1
di-tert-butul 2-(4-[4-(4-[1,3-bis(tert-butoxycarbonyl)tetrahydro-1H-2-imidazolyliden]aminophenyl)piperazino]phenylimino)-1,3-imidazolidinedicarboxylate

Guidance literature:: With triethylamine; mercury dichloride; In N,N-dimethyl-formamide; at 20 ℃; for 60h;
DOI:10.1021/jm031024u

Reference yield:

: 6269-89-2
1-(4-Nitrophenyl)piperazine

: 692259-85-1
di-tert-butul 2-(4-[4-(4-[1,3-bis(tert-butoxycarbonyl)tetrahydro-1H-2-imidazolyliden]aminophenyl)piperazino]phenylimino)-1,3-imidazolidinedicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / dimethylsulfoxide / 60 h / 100 °C

2: 41 percent / HCl; H₂ / Pd/C / methanol / 14 h / 20 °C / 2068.59 Torr

3: 66 percent / Et₃N; HgCl₂ / dimethylformamide / 60 h / 20 °C

With hydrogenchloride; hydrogen; triethylamine; mercury dichloride; palladium on activated charcoal; In methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm031024u

Reference yield:

: 16264-05-4
1,4-bis(4-nitrophenyl)piperazine

: 692259-85-1
di-tert-butul 2-(4-[4-(4-[1,3-bis(tert-butoxycarbonyl)tetrahydro-1H-2-imidazolyliden]aminophenyl)piperazino]phenylimino)-1,3-imidazolidinedicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 41 percent / HCl; H₂ / Pd/C / methanol / 14 h / 20 °C / 2068.59 Torr

2: 66 percent / Et₃N; HgCl₂ / dimethylformamide / 60 h / 20 °C

With hydrogenchloride; hydrogen; triethylamine; mercury dichloride; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm031024u