(+/-)3-azido-2,3-dihydro-1-[4-methoxybenzyl]-2-oxo-5-phenyl-1H-1,4-benzodiazepine

Base Information

Chemical Name:(+/-)3-azido-2,3-dihydro-1-[4-methoxybenzyl]-2-oxo-5-phenyl-1H-1,4-benzodiazepine
CAS No.:174698-36-3
Molecular Formula:C₂₃H₁₉N₅O₂
Molecular Weight:397.436
Hs Code.:

Synonyms:(+/-)3-azido-2,3-dihydro-1-[4-methoxybenzyl]-2-oxo-5-phenyl-1H-1,4-benzodiazepine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)3-azido-2,3-dihydro-1-[4-methoxybenzyl]-2-oxo-5-phenyl-1H-1,4-benzodiazepine

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Technology Process of (+/-)3-azido-2,3-dihydro-1-[4-methoxybenzyl]-2-oxo-5-phenyl-1H-1,4-benzodiazepine

There total 2 articles about (+/-)3-azido-2,3-dihydro-1-[4-methoxybenzyl]-2-oxo-5-phenyl-1H-1,4-benzodiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 36982-84-0
2,4,6-Triisopropylbenzenesulfonyl azide

: 174698-35-2
2,3-dihydro-1-[4-methoxybenzyl]-2-oxo-5-phenyl-1H-1,4-benzodiazepine

: 174698-36-3
(+/-)3-azido-2,3-dihydro-1-[4-methoxybenzyl]-2-oxo-5-phenyl-1H-1,4-benzodiazepine

Guidance literature:: With potassium hexamethylsilazane; In tetrahydrofuran; chloroform; acetic acid; toluene;

Reference yield:

: 174698-35-2
2,3-dihydro-1-[4-methoxybenzyl]-2-oxo-5-phenyl-1H-1,4-benzodiazepine

: 174698-36-3
(+/-)3-azido-2,3-dihydro-1-[4-methoxybenzyl]-2-oxo-5-phenyl-1H-1,4-benzodiazepine

Guidance literature:: With 2,4,6-Triisopropylbenzenesulfonyl azide; potassium hexamethylsilazane; Yield given. Multistep reaction; 1.) THF, toluene, -78 deg C, 5 min; 2.) THF, toluene, -78 deg C, 5 min;
DOI:10.1016/S0040-4039(96)01475-X