C₄₉H₇₀O₇Si

Base Information

Chemical Name:C₄₉H₇₀O₇Si
CAS No.:1449419-37-7
Molecular Formula:C₄₉H₇₀O₇Si
Molecular Weight:799.176
Hs Code.:

C<sub>49</sub>H<sub>70</sub>O<sub>7</sub>Si

Synonyms:C₄₉H₇₀O₇Si

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Chemical Property of C₄₉H₇₀O₇Si

Chemical Property:

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Technology Process of C₄₉H₇₀O₇Si

There total 8 articles about C₄₉H₇₀O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 994-30-9
triethylsilyl chloride

: 1449419-34-4
C₄₃H₅₆O₇

: 1449419-37-7
C₄₉H₇₀O₇Si

Guidance literature:: With 1H-imidazole; In tetrahydrofuran; at 20 ℃; for 4h;
DOI:10.1016/j.tet.2013.02.008

Reference yield:

: 1449419-19-5
C₁₆H₂₄O₃S₂

: 1449419-37-7
C₄₉H₇₀O₇Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran; toluene / 21 h / 0 - 20 °C

2.1: sodium hydroxide / tetrahydrofuran; water; methanol / 12 h / 0 - 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

3.2: 21.5 h / 0 - 20 °C

4.1: sodium hydrogencarbonate; methyl iodide / acetonitrile; water / 19 h / 20 °C

5.1: sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium chlorite / tetrahydrofuran; water; tert-butyl alcohol / 0.5 h / 4 °C

6.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 3 h / 20 °C

6.2: 1.5 h / 50 °C

7.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 1 h / 20 °C

8.1: 1H-imidazole / tetrahydrofuran / 4 h / 20 °C

With 1H-imidazole; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; di-isopropyl azodicarboxylate; 2,4,6-trichlorobenzoyl chloride; sodium hydride; sodium hydrogencarbonate; triethylamine; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; methyl iodide; In tetrahydrofuran; methanol; dichloromethane; water; toluene; acetonitrile; mineral oil; tert-butyl alcohol; 1.1: |Mitsunobu Displacement / 6.1: |Yamaguchi Lactonization / 6.2: |Yamaguchi Lactonization;
DOI:10.1016/j.tet.2013.02.008

Reference yield:

: 1449419-20-8
C₁₆H₂₄O₃S₂

: 1449419-37-7
C₄₉H₇₀O₇Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

1.2: 21.5 h / 0 - 20 °C

2.1: sodium hydrogencarbonate; methyl iodide / acetonitrile; water / 19 h / 20 °C

3.1: sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium chlorite / tetrahydrofuran; water; tert-butyl alcohol / 0.5 h / 4 °C

4.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 3 h / 20 °C

4.2: 1.5 h / 50 °C

5.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 1 h / 20 °C

6.1: 1H-imidazole / tetrahydrofuran / 4 h / 20 °C

With 1H-imidazole; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; 2,4,6-trichlorobenzoyl chloride; sodium hydride; sodium hydrogencarbonate; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; methyl iodide; In tetrahydrofuran; dichloromethane; water; toluene; acetonitrile; mineral oil; tert-butyl alcohol; 4.1: |Yamaguchi Lactonization / 4.2: |Yamaguchi Lactonization;
DOI:10.1016/j.tet.2013.02.008