C₂₈H₂₇NO₆

Base Information

Chemical Name:C₂₈H₂₇NO₆
CAS No.:135144-02-4
Molecular Formula:C₂₈H₂₇NO₆
Molecular Weight:473.525
Hs Code.:

C<sub>28</sub>H<sub>27</sub>NO<sub>6</sub>

Synonyms:C₂₈H₂₇NO₆

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Chemical Property of C₂₈H₂₇NO₆

Chemical Property:

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Technology Process of C₂₈H₂₇NO₆

There total 21 articles about C₂₈H₂₇NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 64-17-5
ethanol

: 135106-77-3,141395-29-1
C₂₆H₁₉NO₅

: 135144-04-6
C₂₆H₁₉NO₆

: 135144-02-4
C₂₈H₂₇NO₆

Guidance literature:: With oxygen; In tetrahydrofuran; at 25 ℃; for 1.5h; phosphate buffer pH 8.0;

Reference yield: 31.0%

: 64-17-5
ethanol

: 135106-77-3,141395-29-1
C₂₆H₁₉NO₅

: 135144-02-4
C₂₈H₂₇NO₆

Guidance literature:: In tetrahydrofuran; at 25 ℃; for 1.5h; phosphate buffer pH 8.0;

Reference yield:

: 144019-65-8
3-(benzyloxy)-7,8,9,10-tetrahydrophenanthridine

: 135144-02-4
C₂₈H₂₇NO₆

Guidance literature:: Multi-step reaction with 15 steps

1: 88 percent / m-CPBA / CH₂Cl₂ / 0.5 h / 25 °C

2: 80 percent / 14 h / 25 °C

3: 98 percent / K₂CO₃ / methanol / 2 h / 25 °C

4: 98 percent / 2,6-lutidine / CH₂Cl₂ / 0.5 h / 25 °C

5: 89 percent / H₂ / 10percent Pd/C / ethanol / 4 h / 760 Torr

6: 1.) NaH, 2.) n-Bu₄NI / 1.) THF, 10 min, 2.) THF, 25 deg C, 1 h

7: 98 percent / tetrahydrofuran / 0.25 h / -78 - 0 °C

8: 1.) Pd(PPh₃)4, n-PrNH₂, 2.) CuI / 1.) benzene, 25 deg C, 15 min, 2.) benzene, 25 deg C, 5 h

9: m-CPBA / CH₂Cl₂ / 1 h / 25 °C

10: 82 percent / 48percent aq. HBr / tetrahydrofuran / 2 h / 25 °C

11: 1.) AgNO₃, 2.) KCN / 1.) THF, EtOH, H₂O, 25 deg C, 1 h, 2.) THF, EtOH, H₂O, 25 deg C, 10 min

12: 59 percent / sat. aq. NaHCO₃, m-CPBA / CH₂Cl₂ / 1 h / 25 °C

13: 42 percent / LDA / toluene; cyclohexane / 0.33 h / -78 °C

14: D₂O / Irradiation

15: aq. potassium phosphate monobasic-sodium hydroxide buffer / tetrahydrofuran / 1.5 h / 25 °C / pH 8.0

With 2,6-dimethylpyridine; propylamine; potassium cyanide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium phosphate monobasic-sodium hydroxide buffer; hydrogen bromide; hydrogen; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium hydrogencarbonate; potassium carbonate; silver nitrate; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; cyclohexane; water-d2; toluene;
DOI:10.1021/ja00049a023