diethylthiocarbamic acid [benzyl(cyclohex-2-enyl)carbamic acid]thioanhydride

Base Information

Chemical Name:diethylthiocarbamic acid [benzyl(cyclohex-2-enyl)carbamic acid]thioanhydride
CAS No.:752203-45-5
Molecular Formula:C₁₉H₂₆N₂OS₂
Molecular Weight:362.56
Hs Code.:

Synonyms:diethylthiocarbamic acid [benzyl(cyclohex-2-enyl)carbamic acid]thioanhydride

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Chemical Property of diethylthiocarbamic acid [benzyl(cyclohex-2-enyl)carbamic acid]thioanhydride

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Technology Process of diethylthiocarbamic acid [benzyl(cyclohex-2-enyl)carbamic acid]thioanhydride

There total 5 articles about diethylthiocarbamic acid [benzyl(cyclohex-2-enyl)carbamic acid]thioanhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 20624-25-3
sodium diethyldithiocarbamate trihydrate

: 1027018-37-6
benzyl(cyclohex-2-enyl)carbamic chloride

: 752203-45-5
diethylthiocarbamic acid [benzyl(cyclohex-2-enyl)carbamic acid]thioanhydride

Guidance literature:: In acetone; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1021/ol300605y

Reference yield:

: 141330-12-3
N-benzyl-N-(2-cyclohexenyl)amine

: 752203-45-5
diethylthiocarbamic acid [benzyl(cyclohex-2-enyl)carbamic acid]thioanhydride

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / toluene / 20 °C

2: acetone / 20 °C

With pyridine; In acetone; toluene;
DOI:10.1002/anie.200453600