6-tert-butoxycarbonylamino-2-trifluoromethansulfonyloxy-hexanoic acid benzyl ester

Base Information

• Chemical Name: 6-tert-butoxycarbonylamino-2-trifluoromethansulfonyloxy-hexanoic acid benzyl ester
• CAS No.: 769969-66-6
• Molecular Formula: C₁₉H₂₆F₃NO₇S
• Molecular Weight: 469.479

Synonyms:6-tert-butoxycarbonylamino-2-trifluoromethansulfonyloxy-hexanoic acid benzyl ester

Chemical Property of 6-tert-butoxycarbonylamino-2-trifluoromethansulfonyloxy-hexanoic acid benzyl ester

Chemical Property:

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Technology Process of 6-tert-butoxycarbonylamino-2-trifluoromethansulfonyloxy-hexanoic acid benzyl ester

There total 1 articles about 6-tert-butoxycarbonylamino-2-trifluoromethansulfonyloxy-hexanoic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C18H27NO5 + trifluoromethylsulfonic anhydride (358-23-6) → 6-tert-butoxycarbonylamino-2-trifluoromethansulfonyloxy-hexanoic acid benzyl ester (769969-66-6)

Guidance literature:

With pyridine; In dichloromethane; at -20 ℃;

Reference yield: 78.8%

6-tert-butoxycarbonylamino-2-trifluoromethansulfonyloxy-hexanoic acid benzyl ester (769969-66-6) + (2R,5S)-5-({[2-(bis-tert-butoxycarbonylmethyl-amino)ethyl]-tert-butoxycarbonylmethyl-amino}methyl)pyrrolidine-2-carboxylic acid ethyl ester (769969-22-4) → (1'R,2R,5S)-1-(1-benzyloxycarbonyl-5-tert-butoxycarbonylamino-pentyl)-5-({[2-(bis-tert-butoxycarbonylmethyl-amino)ethyl]-tert-butoxycarbonylmethyl-amino}methyl)pyrrolidine-2-carboxylic acid ethyl ester

Guidance literature:

In dichloromethane; at -20 - 20 ℃; for 7h;

Reference yield: 78.3%

6-tert-butoxycarbonylamino-2-trifluoromethansulfonyloxy-hexanoic acid benzyl ester (769969-66-6) + (2R,5S)-1-benzyl-5-((diethoxyphosphorylmethyl)-{2-[(diethoxy-phosphorylmethyl)amino]-ethyl}carbamoyl)-pyrrolidine-2-carboxylic acid ethyl ester (769969-37-1) → (1'R,2R,5S)-1-benzyl-5-[{2-[(1-benzyloxycarbonyl-5-tert-butoxycarbonylaminopentyl)-(diethoxyphosphorylmethyl)amino]ethyl}(diethoxyphosphorylmethyl) carbamoyl]pyrrolidine-2-carboxylic acid ethyl ester (769969-38-2)

Guidance literature:

In dichloromethane; at -20 - 20 ℃; for 2h;

upstream raw materials:

trifluoromethylsulfonic anhydride

Downstream raw materials:

(1'R,2R,5S)-1-(1-benzyloxycarbonyl-5-tert-butoxycarbonylamino-pentyl)-5-(tert-butoxycarbonylmethyl-{2-[tert-butoxycarbonylmethyl-(1-ethoxycarbonyl-ethyl)amino]ethyl}carbamoyl)pyrrolidine-2-carboxylic acid ethyl ester

(1'R,1''R,1'''R,2R,5S)-1-benzyl-5-[{2-[(1-benzyloxycarbonyl-5-tert-butoxycarbonylamino-pentyl)(1-ethoxycarbonyl-ethyl)amino]ethyl}(1-ethoxycarbonyl-ethyl)carbamoyl]pyrrolidine-2-carboxylic acid ethyl ester

(1'R,2R,5S)-1-benzyl-5-({2-[(1-benzyloxycarbonyl-5-tert-butoxycarbonylamino-pentyl)-tert-butoxycarbonylmethyl-amino]ethyl}tert-butoxycarbonylmethyl-carbamoyl)pyrrolidine-2-carboxylic acid ethyl ester

(1'R,2R,5S)-1-benzyl-5-[{2-[(1-benzyloxycarbonyl-5-tert-butoxycarbonylaminopentyl)-(diethoxyphosphorylmethyl)amino]ethyl}(diethoxyphosphorylmethyl) carbamoyl]pyrrolidine-2-carboxylic acid ethyl ester

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