C₁₉H₂₄O₈

Base Information

• Chemical Name: C₁₉H₂₄O₈
• CAS No.: 1313593-71-3
• Molecular Formula: C₁₉H₂₄O₈
• Molecular Weight: 380.395
• Mol file: 1313593-71-3.mol

Synonyms:C₁₉H₂₄O₈

Chemical Property of C₁₉H₂₄O₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₉H₂₄O₈

There total 4 articles about C₁₉H₂₄O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C24H30O10 → C19H24O8 (1313593-71-3)

Guidance literature:

With sodium methylate; In methanol; dichloromethane; at 0 - 20 ℃;

DOI:10.1016/j.tetlet.2011.04.060

Reference yield:

ethylthio 4,6-O-benzylidene-2,3-di-O-levulinyl-β-D-glucopyranoside (1259036-06-0) → C19H24O8 (1313593-71-3)

Guidance literature:

Multi-step reaction with 2 steps

1: N-Bromosuccinimide; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.5 h / 0 °C / Molecular sieve

2: sodium methylate / methanol; dichloromethane / 0 - 20 °C

With N-Bromosuccinimide; trimethylsilyl trifluoromethanesulfonate; sodium methylate; In methanol; dichloromethane;

DOI:10.1016/j.tetlet.2011.04.060

Reference yield:

levulinic acid (123-76-2) → C19H24O8 (1313593-71-3)

Guidance literature:

Multi-step reaction with 3 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 42 °C

2: N-Bromosuccinimide; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.5 h / 0 °C / Molecular sieve

3: sodium methylate / methanol; dichloromethane / 0 - 20 °C

With dmap; N-Bromosuccinimide; trimethylsilyl trifluoromethanesulfonate; sodium methylate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane;

DOI:10.1016/j.tetlet.2011.04.060

upstream raw materials:

ethylthio 4,6-O-benzylidene-2,3-di-O-levulinyl-β-D-glucopyranoside

levulinic acid

ethyl 4,6-O-benzylidene-1-thio-β-D-glucopyranoside