(+/-)-1-(4,4-diphenylbutyl)-4-(3-phosphonopropyl)-2-piperazinecarboxylic acid dihydrochloride

Base Information

Chemical Name:(+/-)-1-(4,4-diphenylbutyl)-4-(3-phosphonopropyl)-2-piperazinecarboxylic acid dihydrochloride
CAS No.:129365-47-5
Molecular Formula:C₂₄H₃₃N₂O₅P*2ClH
Molecular Weight:533.432
Hs Code.:

Synonyms:(+/-)-1-(4,4-diphenylbutyl)-4-(3-phosphonopropyl)-2-piperazinecarboxylic acid dihydrochloride

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Chemical Property of (+/-)-1-(4,4-diphenylbutyl)-4-(3-phosphonopropyl)-2-piperazinecarboxylic acid dihydrochloride

Chemical Property:

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Technology Process of (+/-)-1-(4,4-diphenylbutyl)-4-(3-phosphonopropyl)-2-piperazinecarboxylic acid dihydrochloride

There total 4 articles about (+/-)-1-(4,4-diphenylbutyl)-4-(3-phosphonopropyl)-2-piperazinecarboxylic acid dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 126937-41-5
1-(benzyloxycarbonyl)-4-(tert-butoxycarbonyl)-2-piperazinecarboxylic acid

: 129365-47-5
(+/-)-1-(4,4-diphenylbutyl)-4-(3-phosphonopropyl)-2-piperazinecarboxylic acid dihydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / CH₂Cl₂ / 18 h / 25 °C

2: 55 percent / Na₂CO₃ / ethanol / 20 h / Heating

3: 100 percent / H₂ / 20percent Pd/C / ethanol / 4 h

With hydrogen; sodium carbonate; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1021/jm00172a037

Reference yield:

: 1-(phenylmethyl) (+/-)-4-<3-(diethoxyphosphinyl)propyl>-1,2-piperazinedicarboxylate

: 129365-47-5
(+/-)-1-(4,4-diphenylbutyl)-4-(3-phosphonopropyl)-2-piperazinecarboxylic acid dihydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / H₂ / 20percent Pd/C / ethanol / 4 h

With hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00172a037

Reference yield:

: 129365-25-9
1-(phenylmethyl) (+/-)-1,2-piperazinedicarboxylate trifluoroacetate

: 129365-47-5
(+/-)-1-(4,4-diphenylbutyl)-4-(3-phosphonopropyl)-2-piperazinecarboxylic acid dihydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 55 percent / Na₂CO₃ / ethanol / 20 h / Heating

2: 100 percent / H₂ / 20percent Pd/C / ethanol / 4 h

With hydrogen; sodium carbonate; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00172a037