1,2-O-isopropylidene-3-(4-nitrophenoxycarbonyl)-5-methyl-5-deoxy-α-D-xylofuranose

Base Information

Chemical Name:1,2-O-isopropylidene-3-(4-nitrophenoxycarbonyl)-5-methyl-5-deoxy-α-D-xylofuranose
CAS No.:1187322-40-2
Molecular Formula:C₁₅H₁₇NO₈
Molecular Weight:339.302
Hs Code.:

Synonyms:1,2-O-isopropylidene-3-(4-nitrophenoxycarbonyl)-5-methyl-5-deoxy-α-D-xylofuranose

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Chemical Property of 1,2-O-isopropylidene-3-(4-nitrophenoxycarbonyl)-5-methyl-5-deoxy-α-D-xylofuranose

Chemical Property:

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Technology Process of 1,2-O-isopropylidene-3-(4-nitrophenoxycarbonyl)-5-methyl-5-deoxy-α-D-xylofuranose

There total 2 articles about 1,2-O-isopropylidene-3-(4-nitrophenoxycarbonyl)-5-methyl-5-deoxy-α-D-xylofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7693-46-1
4-Nitrophenyl chloroformate

: 4152-79-8,33156-02-4,37105-87-6,37105-91-2,37105-93-4,53597-97-0,97059-40-0
1,2-O-isopropylidene-5-methyl-5-deoxy-α-D-xylofuranose

: 1187322-40-2
1,2-O-isopropylidene-3-(4-nitrophenoxycarbonyl)-5-methyl-5-deoxy-α-D-xylofuranose

Guidance literature:: With triethylamine; In acetonitrile; at 20 - 45 ℃; for 3.16667h;

Reference yield:

: 6893-65-8,20513-95-5,20513-96-6,34981-06-1,40429-51-4,110349-61-6
1,2-di-O-isopropylidene-5-O-tosyl-D-xylofuranose

: 1187322-40-2
1,2-O-isopropylidene-3-(4-nitrophenoxycarbonyl)-5-methyl-5-deoxy-α-D-xylofuranose

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 20 - 80 °C

1.2: 0 - 5 °C

2.1: triethylamine / acetonitrile / 3.17 h / 20 - 45 °C

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; acetonitrile;

Reference yield:

: (4-methyl-piperidin-4-yl)-carbamic acid benzyl ester hydrochloride

: 1187322-40-2
1,2-O-isopropylidene-3-(4-nitrophenoxycarbonyl)-5-methyl-5-deoxy-α-D-xylofuranose

: 1187322-41-3
C₂₃H₃₂N₂O₇

Guidance literature:: (4-methyl-piperidin-4-yl)-carbamic acid benzyl ester hydrochloride; With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; for 0.166667h;

1,2-O-isopropylidene-3-(4-nitrophenoxycarbonyl)-5-methyl-5-deoxy-α-D-xylofuranose; In acetonitrile; at 45 ℃; for 1h;