Carbonic acid 3-dimethylcarbamoyl-1,1-dimethyl-propyl ester 4-nitro-phenyl ester

Base Information

• Chemical Name: Carbonic acid 3-dimethylcarbamoyl-1,1-dimethyl-propyl ester 4-nitro-phenyl ester
• CAS No.: 58939-59-6
• Molecular Formula: C₁₅H₂₀N₂O₆
• Molecular Weight: 324.334
• Mol file: 58939-59-6.mol

Synonyms:Carbonic acid 3-dimethylcarbamoyl-1,1-dimethyl-propyl ester 4-nitro-phenyl ester

Chemical Property of Carbonic acid 3-dimethylcarbamoyl-1,1-dimethyl-propyl ester 4-nitro-phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Carbonic acid 3-dimethylcarbamoyl-1,1-dimethyl-propyl ester 4-nitro-phenyl ester

There total 2 articles about Carbonic acid 3-dimethylcarbamoyl-1,1-dimethyl-propyl ester 4-nitro-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dihydro-5,5-dimethyl-2(3H)-furanone (3123-97-5) → Carbonic acid 3-dimethylcarbamoyl-1,1-dimethyl-propyl ester 4-nitro-phenyl ester (58939-59-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 336 h

2: 4-methyl-morpholine

With 4-methyl-morpholine;

Reference yield:

4-Hydroxy-4-methylvaleriansaeure-dimethylamid (36763-99-2) + 4-Nitrophenyl chloroformate (7693-46-1) → Carbonic acid 3-dimethylcarbamoyl-1,1-dimethyl-propyl ester 4-nitro-phenyl ester (58939-59-6)

Guidance literature:

With 4-methyl-morpholine;

DOI:10.1039/c39750000939

Reference yield:

Carbonic acid 3-dimethylcarbamoyl-1,1-dimethyl-propyl ester 4-nitro-phenyl ester (58939-59-6) + Nα-benzyloxycarbonyl-L-ornithine (2640-58-6) → (S)-2-Benzyloxycarbonylamino-5-(3-dimethylcarbamoyl-1,1-dimethyl-propoxycarbonylamino)-pentanoic acid (72039-36-2)

Guidance literature:

With 1,1,3,3-tetramethylguanidine;

upstream raw materials:

4-Hydroxy-4-methylvaleriansaeure-dimethylamid

4-Nitrophenyl chloroformate

dihydro-5,5-dimethyl-2(3H)-furanone

Downstream raw materials:

(S)-2-Benzyloxycarbonylamino-6-(3-dimethylcarbamoyl-1,1-dimethyl-propoxycarbonylamino)-hexanoic acid

(S)-2-Benzyloxycarbonylamino-5-(3-dimethylcarbamoyl-1,1-dimethyl-propoxycarbonylamino)-pentanoic acid