2-(3,5-dimethylpyrazol-4-yl)carbonylmethylthio-3-cyano-6-(4-hydroxyphenyl)-4-phenylpyridine

Base Information

Chemical Name:2-(3,5-dimethylpyrazol-4-yl)carbonylmethylthio-3-cyano-6-(4-hydroxyphenyl)-4-phenylpyridine
CAS No.:157222-97-4
Molecular Formula:C₂₅H₂₀N₄O₂S
Molecular Weight:440.525
Hs Code.:

Synonyms:2-(3,5-dimethylpyrazol-4-yl)carbonylmethylthio-3-cyano-6-(4-hydroxyphenyl)-4-phenylpyridine

Suppliers and Price of 2-(3,5-dimethylpyrazol-4-yl)carbonylmethylthio-3-cyano-6-(4-hydroxyphenyl)-4-phenylpyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(3,5-dimethylpyrazol-4-yl)carbonylmethylthio-3-cyano-6-(4-hydroxyphenyl)-4-phenylpyridine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(3,5-dimethylpyrazol-4-yl)carbonylmethylthio-3-cyano-6-(4-hydroxyphenyl)-4-phenylpyridine

There total 4 articles about 2-(3,5-dimethylpyrazol-4-yl)carbonylmethylthio-3-cyano-6-(4-hydroxyphenyl)-4-phenylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 157222-95-2
<3-cyano-6-(4-hydroxyphenyl)-4-phenyl-2-pyridylthio>acethydrazide

: 123-54-6,81235-32-7
acetylacetone

: 157222-97-4
2-(3,5-dimethylpyrazol-4-yl)carbonylmethylthio-3-cyano-6-(4-hydroxyphenyl)-4-phenylpyridine

Guidance literature:: In ethanol; for 5h; Heating;
DOI:10.1135/cccc19940978

Reference yield:

: 2657-25-2
(E)-1-(4-hydroxyphenyl)-3-phenylprop-2-en-1-one

: 157222-97-4
2-(3,5-dimethylpyrazol-4-yl)carbonylmethylthio-3-cyano-6-(4-hydroxyphenyl)-4-phenylpyridine

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / Na / methanol / 48 h / 50 °C

2: 89 percent / sodium acetate / ethanol / 3 h / Heating

3: 81 percent / 99percent hydrazine hydrate / ethanol / 4 h / Heating

4: 76 percent / ethanol / 5 h / Heating

With sodium acetate; sodium; hydrazine hydrate; In methanol; ethanol;
DOI:10.1135/cccc19940978

Reference yield:

: 157222-84-9
3-cyano-6-(4-hydroxyphenyl)-2-mercapto-4-phenylpyridine

: 157222-97-4
2-(3,5-dimethylpyrazol-4-yl)carbonylmethylthio-3-cyano-6-(4-hydroxyphenyl)-4-phenylpyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / sodium acetate / ethanol / 3 h / Heating

2: 81 percent / 99percent hydrazine hydrate / ethanol / 4 h / Heating

3: 76 percent / ethanol / 5 h / Heating

With sodium acetate; hydrazine hydrate; In ethanol;
DOI:10.1135/cccc19940978