[2,6-bis(ethoxymethyl)phenyl](triphenyl)tin

Base Information

• Chemical Name: [2,6-bis(ethoxymethyl)phenyl](triphenyl)tin
• CAS No.: 770743-95-8
• Molecular Formula: C₃₀H₃₂O₂Sn
• Molecular Weight: 543.293

Synonyms:[2,6-bis(ethoxymethyl)phenyl](triphenyl)tin

Chemical Property of [2,6-bis(ethoxymethyl)phenyl](triphenyl)tin

Chemical Property:

Purity/Quality:

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Technology Process of [2,6-bis(ethoxymethyl)phenyl](triphenyl)tin

There total 1 articles about [2,6-bis(ethoxymethyl)phenyl](triphenyl)tin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

1,3-bis(ethoxymethyl)benzene + triphenyltin chloride (639-58-7) → [2,6-bis(ethoxymethyl)phenyl](triphenyl)tin (770743-95-8)

Guidance literature:

With n-C₄H₉Li; In hexane; (Ar); using Schlenk techniques; addn. dropwise of equimolar amt. of n-BuLi to soln. of 1,3-bis(ethoxymethyl)benzene in n-hexane at ambient temp.; stirring for 2 h; addn. dropwise to suspn. of Ph3SnCl in n-hexane at room temp.; stirring for 12 h; filtration, washing with n-hexane; concd.; crystn. at -10°C; filtration, elem. anal.;

DOI:10.1021/om700576n

upstream raw materials:

triphenyltin chloride

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