Ru(C_.tplbond.CC₆H₄C_.tplbond.CSiMe₃)(PPh₃)2Cp

Base Information

Chemical Name:Ru(C_.tplbond.CC₆H₄C_.tplbond.CSiMe₃)(PPh₃)2Cp
CAS No.:256391-99-8
Molecular Formula:C₅₄H₄₈P₂RuSi
Molecular Weight:888.078
Hs Code.:

Ru(C<sub>.</sub>tplbond.CC<sub>6</sub>H<sub>4</sub>C<sub>.</sub>tplbond.CSiMe<sub>3</sub>)(PPh<sub>3</sub>)2Cp

Synonyms:Ru(C_.tplbond.CC₆H₄C_.tplbond.CSiMe₃)(PPh₃)2Cp

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Chemical Property of Ru(C_.tplbond.CC₆H₄C_.tplbond.CSiMe₃)(PPh₃)2Cp

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Technology Process of Ru(C_.tplbond.CC₆H₄C_.tplbond.CSiMe₃)(PPh₃)2Cp

There total 2 articles about Ru(C_.tplbond.CC₆H₄C_.tplbond.CSiMe₃)(PPh₃)2Cp which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 32993-05-8
chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II)

: 17938-13-5
1,4-Bis(trimethylsilylethynyl)benzene

: 256391-99-8
Ru(C_.tplbond.CC₆H₄C_.tplbond.CSiMe₃)(PPh₃)2Cp

Guidance literature:: With KF; In methanol; (N2); reflux (overnight); filtration, chromy. (alumina; acetone/hexane), concn., filtration, washing (hexane); elem. anal.;
DOI:10.1039/a905174k

Reference yield: 33.0%

: 32993-05-8
chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II)

: 66228-76-0
4-(trimethylsilylethynyl)phenylacetylene

: 256391-99-8
Ru(C_.tplbond.CC₆H₄C_.tplbond.CSiMe₃)(PPh₃)2Cp

Guidance literature:: With NH₄PF₆; 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU); In methanol; under N2; heated at reflux for 3.5 h, treated with four drops of DBU; ppt. collected by filtration, washed with CH3OH, air-dried;
DOI:10.1016/j.ica.2011.02.043

Reference yield: 97.0%

: 256391-99-8
Ru(C_.tplbond.CC₆H₄C_.tplbond.CSiMe₃)(PPh₃)2Cp

: 670-54-2
ethenetetracarbonitrile

: 257884-86-9
Ru(η(3)-C[=C(CN)2]C(C6H4C.tplbond.CSiMe3)=C(CN)2)(PPh3)Cp

Guidance literature:: In tetrahydrofuran; N2-atmosphere; equimolar amts., refluxing for 3 h; solvent removal, thin layer chromy. (SiO2, Me2CO/hexane=3:7), recrystn. (CH2Cl2/hexane); elem. anal.;
DOI:10.1016/S0022-328X(99)00487-8