(2S,3S)-2-(Benzyloxymethoxy)-3-(benzyloxymethyl)butane-1,4-diyl dimethanesulfonate

Base Information

Chemical Name:(2S,3S)-2-(Benzyloxymethoxy)-3-(benzyloxymethyl)butane-1,4-diyl dimethanesulfonate
CAS No.:853270-47-0
Molecular Formula:C₂₂H₃₀O₉S₂
Molecular Weight:502.607
Hs Code.:

Synonyms:(2S,3S)-2-(Benzyloxymethoxy)-3-(benzyloxymethyl)butane-1,4-diyl dimethanesulfonate

Suppliers and Price of (2S,3S)-2-(Benzyloxymethoxy)-3-(benzyloxymethyl)butane-1,4-diyl dimethanesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2S,3S)-2-(Benzyloxymethoxy)-3-(benzyloxymethyl)butane-1,4-diyl dimethanesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S,3S)-2-(Benzyloxymethoxy)-3-(benzyloxymethyl)butane-1,4-diyl dimethanesulfonate

There total 3 articles about (2S,3S)-2-(Benzyloxymethoxy)-3-(benzyloxymethyl)butane-1,4-diyl dimethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 124-63-0
methanesulfonyl chloride

: 797050-32-9
(2S,3R)-3-benzyloxymethyl-2-benzyloxy-methoxy-1,4-butanediol

: 853270-47-0
(2S,3S)-2-(Benzyloxymethoxy)-3-(benzyloxymethyl)butane-1,4-diyl dimethanesulfonate

Guidance literature:: In pyridine; at 0 - 20 ℃;
DOI:10.1016/j.tetlet.2005.03.077

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 853270-47-0
(2S,3S)-2-(Benzyloxymethoxy)-3-(benzyloxymethyl)butane-1,4-diyl dimethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / LDA; HMPA / tetrahydrofuran; hexane / 30 h / -78 - 20 °C

2: 76 percent / LiAlH₄ / tetrahydrofuran / 4 h / Heating

3: 62 percent / pyridine / 0 - 20 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; lithium diisopropyl amide; In tetrahydrofuran; pyridine; hexane;
DOI:10.1016/j.tetlet.2005.03.077

Reference yield:

: 383368-52-3
diethyl (2S,3R)-3-benzoyloxymethyl-2-benzyloxymethoxysuccinate

: 853270-47-0
(2S,3S)-2-(Benzyloxymethoxy)-3-(benzyloxymethyl)butane-1,4-diyl dimethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / LiAlH₄ / tetrahydrofuran / 4 h / Heating

2: 62 percent / pyridine / 0 - 20 °C

With lithium aluminium tetrahydride; In tetrahydrofuran; pyridine;
DOI:10.1016/j.tetlet.2005.03.077