methyl 3-(methoxycarbonyl)-1-phenyl-1,2,3,4-tetrahydro-naphthalene-2-carboxylate

Base Information

• Chemical Name: methyl 3-(methoxycarbonyl)-1-phenyl-1,2,3,4-tetrahydro-naphthalene-2-carboxylate
• CAS No.: 98678-39-8
• Molecular Formula: C₂₀H₂₀O₄
• Molecular Weight: 324.376

Synonyms:methyl 3-(methoxycarbonyl)-1-phenyl-1,2,3,4-tetrahydro-naphthalene-2-carboxylate

Chemical Property of methyl 3-(methoxycarbonyl)-1-phenyl-1,2,3,4-tetrahydro-naphthalene-2-carboxylate

Chemical Property:

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Technology Process of methyl 3-(methoxycarbonyl)-1-phenyl-1,2,3,4-tetrahydro-naphthalene-2-carboxylate

There total 12 articles about methyl 3-(methoxycarbonyl)-1-phenyl-1,2,3,4-tetrahydro-naphthalene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

4-Phenyl-1,4-dihydro-benzo[d][1,2]oxathiine 3-oxide (95539-08-5) + dimethyl cis-but-2-ene-1,4-dioate (624-48-6) → methyl 3-(methoxycarbonyl)-1-phenyl-1,2,3,4-tetrahydro-naphthalene-2-carboxylate (98678-39-8)

Guidance literature:

In cyclohexane; at 80 ℃; for 5.5h;

DOI:10.1021/jo00224a035

Reference yield: 57.0%

1-hydroxy-4 phenyl-1,3-dihydrobenzothiophene-2,2-dioxide (95539-05-2) + dimethyl cis-but-2-ene-1,4-dioate (624-48-6) → methyl 3-(methoxycarbonyl)-1-phenyl-1,2,3,4-tetrahydro-naphthalene-2-carboxylate (98678-39-8)

Guidance literature:

In cyclohexane; Heating;

DOI:10.1016/S0040-4039(01)81585-9

Reference yield:

trans 2,3-bis(methoxycarbonyl)-1-phenyl-1,2-dihydronaphthalene (98678-45-6) → 2,3-bis(methoxycarbonyl)-1-phenyl-1,2,3,4-tetrahydronaphthalene (98678-40-1) + methyl 3-(methoxycarbonyl)-1-phenyl-1,2,3,4-tetrahydro-naphthalene-2-carboxylate (98678-39-8)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; at 20 ℃; for 18h;

upstream raw materials:

diazomethane

methanol

(+/-)-1r-phenyl-1,2,3,4-tetrahydro-naphthalene-dicarboxylic acid-(2t.3t)

4-Phenyl-1,4-dihydro-benzo[d][1,2]oxathiine 3-oxide

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