Technology Process of C36H36O8
There total 5 articles about C36H36O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
water; acetonitrile;
at 20 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate / dimethyl sulfoxide / 2 h / Heating / reflux
2.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C
2.2: 22 h / 20 °C
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C
4.1: oxygen; methylene blue / tetrahydrofuran; acetonitrile / 11 h / -10 - 0 °C / Irradiation
5.1: hydrogenchloride / water; acetonitrile / 1 h / 20 °C
With
hydrogenchloride; lithium aluminium tetrahydride; oxygen; methylene blue; sodium hydride; potassium carbonate;
In
tetrahydrofuran; water; dimethyl sulfoxide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C
1.2: 22 h / 20 °C
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C
3.1: oxygen; methylene blue / tetrahydrofuran; acetonitrile / 11 h / -10 - 0 °C / Irradiation
4.1: hydrogenchloride / water; acetonitrile / 1 h / 20 °C
With
hydrogenchloride; lithium aluminium tetrahydride; oxygen; methylene blue; sodium hydride;
In
tetrahydrofuran; water; acetonitrile;