4-(4-n-hexadecyloxybenzoyloxy)carboxylic-4-trimethylsilylethynylphenyl ester

Base Information

Chemical Name:4-(4-n-hexadecyloxybenzoyloxy)carboxylic-4-trimethylsilylethynylphenyl ester
CAS No.:1562688-57-6
Molecular Formula:C₄₁H₅₄O₅Si
Molecular Weight:654.962
Hs Code.:

Synonyms:4-(4-n-hexadecyloxybenzoyloxy)carboxylic-4-trimethylsilylethynylphenyl ester

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Chemical Property of 4-(4-n-hexadecyloxybenzoyloxy)carboxylic-4-trimethylsilylethynylphenyl ester

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Technology Process of 4-(4-n-hexadecyloxybenzoyloxy)carboxylic-4-trimethylsilylethynylphenyl ester

There total 3 articles about 4-(4-n-hexadecyloxybenzoyloxy)carboxylic-4-trimethylsilylethynylphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 194663-08-6
4-(4-(hexadecyloxy)benzoyloxy)benzoic acid

: 88075-18-7
4-(2-(trimethylsilyl)ethynyl)phenol

: 1562688-57-6
4-(4-n-hexadecyloxybenzoyloxy)carboxylic-4-trimethylsilylethynylphenyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 0.75h;
DOI:10.1080/15421406.2013.822299

Reference yield:

: 540-38-5
p-Iodophenol

: 1562688-57-6
4-(4-n-hexadecyloxybenzoyloxy)carboxylic-4-trimethylsilylethynylphenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: copper(II) acetate monohydrate; palladium dichloride; triethylamine / 24.5 h / 80 °C / Inert atmosphere

2: dicyclohexyl-carbodiimide; dmap / dichloromethane / 0.75 h / 20 °C

With dmap; copper(II) acetate monohydrate; triethylamine; dicyclohexyl-carbodiimide; palladium dichloride; In dichloromethane; 1: |Sonogashira Cross-Coupling;
DOI:10.1080/15421406.2013.822299

Reference yield:

: 1066-54-2
trimethylsilylacetylene

: 1562688-57-6
4-(4-n-hexadecyloxybenzoyloxy)carboxylic-4-trimethylsilylethynylphenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: copper(II) acetate monohydrate; palladium dichloride; triethylamine / 24.5 h / 80 °C / Inert atmosphere

2: dicyclohexyl-carbodiimide; dmap / dichloromethane / 0.75 h / 20 °C

With dmap; copper(II) acetate monohydrate; triethylamine; dicyclohexyl-carbodiimide; palladium dichloride; In dichloromethane; 1: |Sonogashira Cross-Coupling;
DOI:10.1080/15421406.2013.822299