<3S-(3α,4β,5β)>-5-Benzyloxy-1-hydroxymethyl-3,4-di(methoxymethoxy)-1-cyclopentene

Base Information

Chemical Name:<3S-(3α,4β,5β)>-5-Benzyloxy-1-hydroxymethyl-3,4-di(methoxymethoxy)-1-cyclopentene
CAS No.:159517-68-7
Molecular Formula:C₁₇H₂₄O₆
Molecular Weight:324.374
Hs Code.:

Synonyms:<3S-(3α,4β,5β)>-5-Benzyloxy-1-hydroxymethyl-3,4-di(methoxymethoxy)-1-cyclopentene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <3S-(3α,4β,5β)>-5-Benzyloxy-1-hydroxymethyl-3,4-di(methoxymethoxy)-1-cyclopentene

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Technology Process of <3S-(3α,4β,5β)>-5-Benzyloxy-1-hydroxymethyl-3,4-di(methoxymethoxy)-1-cyclopentene

There total 3 articles about <3S-(3α,4β,5β)>-5-Benzyloxy-1-hydroxymethyl-3,4-di(methoxymethoxy)-1-cyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 159517-67-6
<3S-(3α,4β,5β)>-5-Benzyloxy-1-tert-butyldimethylsilyloxymethyl-3,4-di(methoxymethoxy)-1-cyclopentene

: 159517-68-7
<3S-(3α,4β,5β)>-5-Benzyloxy-1-hydroxymethyl-3,4-di(methoxymethoxy)-1-cyclopentene

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.7164/antibiotics.47.932

Reference yield:

: 100-39-0
benzyl bromide

: 159517-68-7
<3S-(3α,4β,5β)>-5-Benzyloxy-1-hydroxymethyl-3,4-di(methoxymethoxy)-1-cyclopentene

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / NaH / dimethylformamide / 2 h / 0 °C

2: 91 percent / n-Bu₄NF / tetrahydrofuran / 1 h / 0 °C

With tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.7164/antibiotics.47.932

Reference yield:

: 144901-13-3
<1S-(1α,4β,5α)>-2-<<(tert-Butyldimethylsilyl)oxy>methyl>-4,5-bis(methoxymethoxy)-2-cyclopenten-1-ol

: 159517-68-7
<3S-(3α,4β,5β)>-5-Benzyloxy-1-hydroxymethyl-3,4-di(methoxymethoxy)-1-cyclopentene

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / NaH / dimethylformamide / 2 h / 0 °C

2: 91 percent / n-Bu₄NF / tetrahydrofuran / 1 h / 0 °C

With tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.7164/antibiotics.47.932