3-(6-Methoxynaphthalen-2-yl)benzaldehyde

Base Information

Chemical Name:3-(6-Methoxynaphthalen-2-yl)benzaldehyde
CAS No.:237069-42-0
Molecular Formula:C18H14 O2
Molecular Weight:262.3
Hs Code.:2912499000
Mol file:237069-42-0.mol

Synonyms:2-(3-formylphenyl)-6-methoxynaphthalene;3-(6-Methoxy-naphthalen-2-yl)-benzaldehyde;Benzaldehyde,3-(6-methoxy-2-naphthalenyl);

Suppliers and Price of 3-(6-Methoxynaphthalen-2-yl)benzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
3-(6-Methoxynaphthalen-2-yl)benzaldehyde 97%
1g
$ 653.00

Chemenu
3-(6-Methoxynaphthalen-2-yl)benzaldehyde 97%
1g
$ 616.00

American Custom Chemicals Corporation
3-(6-METHOXY-NAPHTHALEN-2-YL)BENZALDEHYDE 95.00%
5MG
$ 497.42

Total 1 raw suppliers

Chemical Property of 3-(6-Methoxynaphthalen-2-yl)benzaldehyde

Chemical Property:

PSA：26.30000
LogP:4.32790

Purity/Quality:: 3-(6-Methoxynaphthalen-2-yl)benzaldehyde 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-(6-Methoxynaphthalen-2-yl)benzaldehyde

There total 7 articles about 3-(6-Methoxynaphthalen-2-yl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 3132-99-8
m-bromobenzoic aldehyde

: 156641-98-4
(6-methoxy-2-naphthalene)boronic acid

: 237069-42-0
3-(6-methoxynaphthalen-2-yl)benzaldehyde

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; for 16h; Heating;
DOI:10.1016/j.bmcl.2007.10.079

Reference yield:

: 5111-65-9
2-Bromo-6-methoxynaphthalene

: 87199-16-4
3-Formylphenylboronic acid

: 237069-42-0
3-(6-methoxynaphthalen-2-yl)benzaldehyde

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; water; toluene; at 80 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.bmc.2022.116615

Reference yield:

: 17789-14-9
3-(1,3-dioxolan-2-yl)-phenylbromide

: 237069-42-0
3-(6-methoxynaphthalen-2-yl)benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 1) Mg, I₂ / 2) Pd(PPh₃)4 / 1) THF, reflux, 2 h, 2) THF, reflux, 2 h

2: aq. HCl / tetrahydrofuran / 10 h / Ambient temperature

With hydrogenchloride; iodine; magnesium; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran;
DOI:10.1002/(SICI)1521-4184(19991)332:1<25::AID-ARDP25>3.0.CO;2-7