9-(5,6-Didesoxy-2,3-O-isopropyliden-6-diphenoxyphosphoryl-β-D-ribo-hex-5-enofuranosyl)adenin

Base Information

Chemical Name:9-(5,6-Didesoxy-2,3-O-isopropyliden-6-diphenoxyphosphoryl-β-D-ribo-hex-5-enofuranosyl)adenin
CAS No.:89301-78-0
Molecular Formula:C₂₆H₂₆N₅O₆P
Molecular Weight:535.496
Hs Code.:

Synonyms:9-(5,6-Didesoxy-2,3-O-isopropyliden-6-diphenoxyphosphoryl-β-D-ribo-hex-5-enofuranosyl)adenin

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Chemical Property of 9-(5,6-Didesoxy-2,3-O-isopropyliden-6-diphenoxyphosphoryl-β-D-ribo-hex-5-enofuranosyl)adenin

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Technology Process of 9-(5,6-Didesoxy-2,3-O-isopropyliden-6-diphenoxyphosphoryl-β-D-ribo-hex-5-enofuranosyl)adenin

There total 3 articles about 9-(5,6-Didesoxy-2,3-O-isopropyliden-6-diphenoxyphosphoryl-β-D-ribo-hex-5-enofuranosyl)adenin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 362-75-4
2',3'-isopropylidene adenosine

: 89301-78-0
9-(5,6-Didesoxy-2,3-O-isopropyliden-6-diphenoxyphosphoryl-β-D-ribo-hex-5-enofuranosyl)adenin

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexylcarbodiimide, trifluoroacetic acid / dimethylsulfoxide; pyridine / 10 h / Ambient temperature

2: dimethylsulfoxide / 48 h / 40 °C

With dicyclohexyl-carbodiimide; trifluoroacetic acid; In pyridine; dimethyl sulfoxide;

Reference yield:

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 89301-78-0
9-(5,6-Didesoxy-2,3-O-isopropyliden-6-diphenoxyphosphoryl-β-D-ribo-hex-5-enofuranosyl)adenin

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 15percent n-butyllithium / 1) THF, n-hexane, 3 h, room temperature, 2) 1 h, room temperature

2: dimethylsulfoxide / 48 h / 40 °C

With n-butyllithium; In dimethyl sulfoxide;