((3aS,6R,6aR)-6-Benzyloxymethyl-6,6a-dihydro-3aH-cyclopentaoxazol-2-yl)-dimethyl-amine

Base Information

Chemical Name:((3aS,6R,6aR)-6-Benzyloxymethyl-6,6a-dihydro-3aH-cyclopentaoxazol-2-yl)-dimethyl-amine
CAS No.:184179-64-4
Molecular Formula:C₁₆H₂₀N₂O₂
Molecular Weight:272.347
Hs Code.:

Synonyms:((3aS,6R,6aR)-6-Benzyloxymethyl-6,6a-dihydro-3aH-cyclopentaoxazol-2-yl)-dimethyl-amine

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Chemical Property of ((3aS,6R,6aR)-6-Benzyloxymethyl-6,6a-dihydro-3aH-cyclopentaoxazol-2-yl)-dimethyl-amine

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Technology Process of ((3aS,6R,6aR)-6-Benzyloxymethyl-6,6a-dihydro-3aH-cyclopentaoxazol-2-yl)-dimethyl-amine

There total 7 articles about ((3aS,6R,6aR)-6-Benzyloxymethyl-6,6a-dihydro-3aH-cyclopentaoxazol-2-yl)-dimethyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100021-11-2
(1α,2β,3α)-2-(benzyloxymethyl)cyclopent-4-ene-1,3-diol

: 184179-64-4
((3aS,6R,6aR)-6-Benzyloxymethyl-6,6a-dihydro-3aH-cyclopentaoxazol-2-yl)-dimethyl-amine

Guidance literature:: Multi-step reaction with 7 steps

1: 89 percent / triethylamine, DMAP / CH₂Cl₂ / 1 h

2: 95 percent / NaH₂PO₄ buffer, aq. sodium azide / 144 h / electric eel acetylcholinesterase

3: pyridine

4: methanolic ammonia

5: K₂CO₃

6: 60 percent / trifluoroacetic anhydride, Et₃N / tetrahydrofuran / -78 - 20 °C

7: 1.) MeOTf / 1.) CH₂Cl₂

With pyridine; dmap; sodium azide; NaH₂PO₄ buffer; ammonia; potassium carbonate; triethylamine; trifluoroacetic anhydride; methyl trifluoromethanesulfonate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja960526c

Reference yield:

: 134756-62-0
<1(S)-(1α,4α,5β)>-4-(acetyloxy)-5-<(benzyloxy)methyl>-2-cyclopenten-1-ol

: 184179-64-4
((3aS,6R,6aR)-6-Benzyloxymethyl-6,6a-dihydro-3aH-cyclopentaoxazol-2-yl)-dimethyl-amine

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine

2: methanolic ammonia

3: K₂CO₃

4: 60 percent / trifluoroacetic anhydride, Et₃N / tetrahydrofuran / -78 - 20 °C

5: 1.) MeOTf / 1.) CH₂Cl₂

With pyridine; ammonia; potassium carbonate; triethylamine; trifluoroacetic anhydride; methyl trifluoromethanesulfonate; In tetrahydrofuran;
DOI:10.1021/ja960526c

Reference yield:

: 134756-61-9
(1α,2β,3α)-2-<(benzyloxy)methyl>-4-cyclopentene-1,3-diol diacetate

: 184179-64-4
((3aS,6R,6aR)-6-Benzyloxymethyl-6,6a-dihydro-3aH-cyclopentaoxazol-2-yl)-dimethyl-amine

Guidance literature:: Multi-step reaction with 6 steps

1: 95 percent / NaH₂PO₄ buffer, aq. sodium azide / 144 h / electric eel acetylcholinesterase

2: pyridine

3: methanolic ammonia

4: K₂CO₃

5: 60 percent / trifluoroacetic anhydride, Et₃N / tetrahydrofuran / -78 - 20 °C

6: 1.) MeOTf / 1.) CH₂Cl₂

With pyridine; sodium azide; NaH₂PO₄ buffer; ammonia; potassium carbonate; triethylamine; trifluoroacetic anhydride; methyl trifluoromethanesulfonate; In tetrahydrofuran;
DOI:10.1021/ja960526c