trans-4-aminocyclohexyl (1S,2R,3S,4S,6R,7R,8R)-4-ethenyl-3-hydroxy-2,4,7,14-tetramethyl-9-oxotricyclo[5.4.3.0(1,8)]tetradec-6-yl imidodicarbonate

Base Information

Chemical Name:trans-4-aminocyclohexyl (1S,2R,3S,4S,6R,7R,8R)-4-ethenyl-3-hydroxy-2,4,7,14-tetramethyl-9-oxotricyclo[5.4.3.0(1,8)]tetradec-6-yl imidodicarbonate
CAS No.:937369-81-8
Molecular Formula:C₂₈H₄₄N₂O₆
Molecular Weight:504.667
Hs Code.:

Synonyms:trans-4-aminocyclohexyl (1S,2R,3S,4S,6R,7R,8R)-4-ethenyl-3-hydroxy-2,4,7,14-tetramethyl-9-oxotricyclo[5.4.3.0(1,8)]tetradec-6-yl imidodicarbonate

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Chemical Property of trans-4-aminocyclohexyl (1S,2R,3S,4S,6R,7R,8R)-4-ethenyl-3-hydroxy-2,4,7,14-tetramethyl-9-oxotricyclo[5.4.3.0(1,8)]tetradec-6-yl imidodicarbonate

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Technology Process of trans-4-aminocyclohexyl (1S,2R,3S,4S,6R,7R,8R)-4-ethenyl-3-hydroxy-2,4,7,14-tetramethyl-9-oxotricyclo[5.4.3.0(1,8)]tetradec-6-yl imidodicarbonate

There total 3 articles about trans-4-aminocyclohexyl (1S,2R,3S,4S,6R,7R,8R)-4-ethenyl-3-hydroxy-2,4,7,14-tetramethyl-9-oxotricyclo[5.4.3.0(1,8)]tetradec-6-yl imidodicarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 937369-86-3
trans-4-({[(1,1-dimethylethyl)oxy]carbonyl}amino)cyclohexyl (1R,2R,4S,6R,7R,9R)-4-ethenyl-2,4,7,14-tetramethyl-9-(methyloxy)-3-oxotricyclo[5.4.3.0(1,8)]tetradec-6-yl imidodicarbonate

: 937369-81-8
trans-4-aminocyclohexyl (1S,2R,3S,4S,6R,7R,8R)-4-ethenyl-3-hydroxy-2,4,7,14-tetramethyl-9-oxotricyclo[5.4.3.0(1,8)]tetradec-6-yl imidodicarbonate

Guidance literature:: trans-4-({[(1,1-dimethylethyl)oxy]carbonyl}amino)cyclohexyl (1R,2R,4S,6R,7R,9R)-4-ethenyl-2,4,7,14-tetramethyl-9-(methyloxy)-3-oxotricyclo[5.4.3.0(1,8)]tetradec-6-yl imidodicarbonate; With hydrogenchloride; water; In toluene; at 10 - 25 ℃; for 2.5h; Large scale reaction;

With ammonium hydroxide; In water; ethyl acetate; isopropyl alcohol; at 15 - 30 ℃; for 2h; Large scale reaction;
DOI:10.1021/op900104g

Reference yield:

: C₃₄H₅₄N₂O₈

: 937369-81-8
trans-4-aminocyclohexyl (1S,2R,3S,4S,6R,7R,8R)-4-ethenyl-3-hydroxy-2,4,7,14-tetramethyl-9-oxotricyclo[5.4.3.0(1,8)]tetradec-6-yl imidodicarbonate

Guidance literature:: C₃₄H₅₄N₂O₈; With hydrogenchloride; In 1,4-dioxane; water; at 0 - 20 ℃; for 2.08333 - 2.58333h;

With ammonia; In water; at 0 - 10 ℃; pH=8.5; Product distribution / selectivity;

Reference yield:

: C₃₅H₅₁F₃N₂O₉

: 937369-81-8
trans-4-aminocyclohexyl (1S,2R,3S,4S,6R,7R,8R)-4-ethenyl-3-hydroxy-2,4,7,14-tetramethyl-9-oxotricyclo[5.4.3.0(1,8)]tetradec-6-yl imidodicarbonate

Guidance literature:: C₃₅H₅₁F₃N₂O₉; With ammonia; In ethanol; water; at 20 ℃; for 3.33333h;

With hydrogenchloride; In 1,4-dioxane; water; at 40 ℃; for 1.5h;

With ammonia; In water; at 0 - 10 ℃; pH=8 - 9; Product distribution / selectivity;