(-)-methylphenyl(triphenylgermyl)methoxysilane

Base Information

• Chemical Name: (-)-methylphenyl(triphenylgermyl)methoxysilane
• CAS No.: 86962-17-6
• Molecular Formula: C₂₆H₂₆GeOSi
• Molecular Weight: 455.167
• Mol file: 86962-17-6.mol

Synonyms:(-)-methylphenyl(triphenylgermyl)methoxysilane

Chemical Property of (-)-methylphenyl(triphenylgermyl)methoxysilane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (-)-methylphenyl(triphenylgermyl)methoxysilane

There total 1 articles about (-)-methylphenyl(triphenylgermyl)methoxysilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

(+)-methylphenyl(triphenylgermyl)chlorosilane (86962-16-5) → (-)-methylphenyl(triphenylgermyl)methoxysilane (86962-17-6)

Guidance literature:

With methanol; cyclohexylamine; In diethyl ether; to a soln. of silane a mixture of methanol and cyclohexylamine was added dropwise at room temp., N2 atm.; filtration, evapn. in vac., recrystn. (pentane);

DOI:10.1016/S0022-328X(00)98846-6

Reference yield: 94.0%

(-)-methylphenyl(triphenylgermyl)methoxysilane (86962-17-6) → (+)-methylphenyl(triphenylgermyl)silane (86962-15-4)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; to a soln. of LiAlH4 silane was added, room temp., 5 min, N2 atm.; hydrolysis, extn., evapn. in vac.;

DOI:10.1016/S0022-328X(00)98846-6

Reference yield: 94.0%

(-)-methylphenyl(triphenylgermyl)methoxysilane (86962-17-6) → (-)-methylphenyl(triphenylgermyl)silane (86962-06-3)

Guidance literature:

With aluminium hydride; In diethyl ether; to a soln. of AlH3 silane was added, room temp., 1 h, N2 atm.; hydrolysis, extn., evapn. in vac.;

DOI:10.1016/S0022-328X(00)98846-6

upstream raw materials:

(+)-methylphenyl(triphenylgermyl)chlorosilane

Downstream raw materials:

(+)-methylphenyl(triphenylgermyl)silane

(-)-methylphenyl(triphenylgermyl)silane

(+)-methylphenyl(triphenylgermyl)fluorosilane